An Efficient Synthesis of 1-Substituted 5-Bromo-1H-tetrazoles

Result code in IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11160%2F13%3A10145937" target="_blank" >RIV/00216208:11160/13:10145937 - isvavai.cz</a>

Result on the web

<a href="https://www.thieme-connect.de/ejournals/html/10.1055/s-0033-1338935" target="_blank" >https://www.thieme-connect.de/ejournals/html/10.1055/s-0033-1338935</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1055/s-0033-1338935" target="_blank" >10.1055/s-0033-1338935</a>

Result language

angličtina

Original language name

An Efficient Synthesis of 1-Substituted 5-Bromo-1H-tetrazoles

Original language description

1-Substituted 1H-tetrazole-5-thiols were efficiently converted into the corresponding 1-substituted 5-bromo-1H-tetrazoles by treatment with zinc(II) bromide and 50% hydrogen peroxide or 36% peracetic acid at 70-80 degrees C. In most cases, the 5-bromotetrazole products could be isolated simply by dilution of the reaction mixture with water followed by filtration and washing of the precipitated product. Column chromatography was needed only in the case of one tetrazole that was additionally brominated onits side chain under the reaction conditions.

Czech name

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Czech description

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Type

J_x - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

CEP classification

CC - Organic chemistry

OECD FORD branch

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Project

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Continuities

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Publication year

2013

Confidentiality

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical

Synthesis

ISSN

0039-7881

e-ISSN

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Volume of the periodical

45

Issue of the periodical within the volume

14

Country of publishing house

DE - GERMANY

Number of pages

5

Pages from-to

2029-2033

UT code for WoS article

000321612300015

EID of the result in the Scopus database

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