Novel Dispersed Sorbent Sorptive Extraction Method for the Chromatography Profiling of Active Substances in Ginger
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11160%2F17%3A10365196" target="_blank" >RIV/00216208:11160/17:10365196 - isvavai.cz</a>
Result on the web
<a href="http://link.springer.com/article/10.1007/s12161-016-0662-8" target="_blank" >http://link.springer.com/article/10.1007/s12161-016-0662-8</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1007/s12161-016-0662-8" target="_blank" >10.1007/s12161-016-0662-8</a>
Alternative languages
Result language
angličtina
Original language name
Novel Dispersed Sorbent Sorptive Extraction Method for the Chromatography Profiling of Active Substances in Ginger
Original language description
One of the important aspects of sample pretreatment is the pre-concentration step. In a sample, analytes are often present in trace levels and pretreatment procedures with high enrichment factor are needed. This work describes the practical aspects of novel dispersed sorbent sorptive extraction (DSSE) method that uses dispersed sorbent for analyte extraction and not for matrix suppression as is typical in QuEChERS. The DSSE was used for the extraction of gingerols, family of active substances in ginger samples, before fast HPLC separation. Using presented extraction method, a high pre-concentration factor (up to 50) of analytes was reached. The separation method using fused-core phenyl-hexyl stationary phase and mobile phase composed of 50 % acetonitrile in water in isocratic mode was developed and validated. Advantages and disadvantages of DSSE and pitfalls during the method development and optimization will be discussed.
Czech name
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Czech description
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Classification
Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
30104 - Pharmacology and pharmacy
Result continuities
Project
<a href="/en/project/GA15-10781S" target="_blank" >GA15-10781S: On-line hyphenation of automated extraction processes with liquid chromatography for complete sample analysis</a><br>
Continuities
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)
Others
Publication year
2017
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Food Analytical Methods
ISSN
1936-9751
e-ISSN
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Volume of the periodical
10
Issue of the periodical within the volume
4
Country of publishing house
US - UNITED STATES
Number of pages
8
Pages from-to
1016-1023
UT code for WoS article
000396148000019
EID of the result in the Scopus database
2-s2.0-84988700538