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Total Description of Intrinsic Amphiphile Aggregation: Calorimetry Study and Molecular Probing

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F18%3A10386108" target="_blank" >RIV/00216208:11310/18:10386108 - isvavai.cz</a>

  • Alternative codes found

    RIV/61389013:_____/18:00497397

  • Result on the web

    <a href="https://doi.org/10.1021/acs.langmuir.8b03462" target="_blank" >https://doi.org/10.1021/acs.langmuir.8b03462</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1021/acs.langmuir.8b03462" target="_blank" >10.1021/acs.langmuir.8b03462</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Total Description of Intrinsic Amphiphile Aggregation: Calorimetry Study and Molecular Probing

  • Original language description

    Isothermal titration calorimetry (ITC) is an apt tool for a total thermodynamic description of self-assembly of atypical amphiphiles such as anionic boron cluster compounds (COSAN) in water. Global fitting of ITC enthalpograms reveals remarkable features that differentiate COSAN from classical amphiphiles: (i) strong enthalpy and weak entropy contribution to the free energy of aggregation, (ii) low degree of counterion binding, and (iii) very low aggregation number, leading to deviations from the ideal closed association model. The counterion condensation obtained from the thermodynamic model was compared with the results of 7Li DOSY NMR of Li[COSAN] micelles, which allows direct tracking of Li cations. The basic thermodynamic study of COSAN alkaline salt aggregation was complemented by NMR and ITC experiments in dilute Li/NaCl and acetonitrile aqueous solutions of COSAN. The strong affinity of acetonitrile molecules to COSAN clusters was microscopically investigated by all-atomic molecular dynamics simulations. The impact of ionic strength on COSAN self-assembling was comparable whereas even a small amount of acetonitrile cosolvent has a pronounced nonclassical character demonstrates that large self-assembling changes are triggered by traces of organic solvents. to the behavior of classical amphiphiles, of COSAN aggregation. It demonstrates that large self-assembling changes are triggered by traces of organic solvents.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10403 - Physical chemistry

Result continuities

  • Project

    <a href="/en/project/GA17-00648S" target="_blank" >GA17-00648S: Chaotrope, hydrotrope or surfactant? Anionic boron cluster compounds in water and in complexes with polymers</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2018

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Langmuir: the ACS journal of surfaces and colloids

  • ISSN

    0743-7463

  • e-ISSN

  • Volume of the periodical

    34

  • Issue of the periodical within the volume

    47

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    10

  • Pages from-to

    14448-14457

  • UT code for WoS article

    000451789300037

  • EID of the result in the Scopus database

    2-s2.0-85056887024