Authentication of two eighteenth century juniper-containing drug remains by HPLC–MS/MS and GC–MSHPLC-MS/MS and GC-MS
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F23%3A10471553" target="_blank" >RIV/00216208:11310/23:10471553 - isvavai.cz</a>
Result on the web
<a href="https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=mQSS9p54C9" target="_blank" >https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=mQSS9p54C9</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1007/s00706-023-03096-x" target="_blank" >10.1007/s00706-023-03096-x</a>
Alternative languages
Result language
angličtina
Original language name
Authentication of two eighteenth century juniper-containing drug remains by HPLC–MS/MS and GC–MSHPLC-MS/MS and GC-MS
Original language description
Two historical remains of juniper-containing drugs, dating from the eighteenth century, were analyzed using two separation techniques with mass detection (HPLC-MS/MS and GC-MS). As reference material, replicates of one of these analyzed historical remains, juniper preserve, were prepared according to period recipes. Although the HPLC-MS/MS method was suitable for authenticating the origin of a drug prepared from juniper berries (i.e., juniper preserve), it proved unsuitable for a drug containing only juniper wood. In contrast, GC-MS was able to demonstrate that this drug did indeed contain juniper wood. Thus both studied samples were verified to be juniper-containing drugs. A remarkable stability of some glycosides was observed in the samples analyzed. The presence of viridiflorin was demonstrated for the first time in the juniper plant, and a detailed ESI+-MSn fragmentation of this substance was proposed.
Czech name
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Czech description
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Classification
Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10406 - Analytical chemistry
Result continuities
Project
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Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Others
Publication year
2023
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Monatshefte für Chemie - Chemical Monthly
ISSN
0026-9247
e-ISSN
1434-4475
Volume of the periodical
154
Issue of the periodical within the volume
9
Country of publishing house
AT - AUSTRIA
Number of pages
10
Pages from-to
977-986
UT code for WoS article
001028718100002
EID of the result in the Scopus database
2-s2.0-85164465327