Shedding electrons on ADOR zeolite structures – Structure determination by 3DED
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F25%3A10497894" target="_blank" >RIV/00216208:11310/25:10497894 - isvavai.cz</a>
Result on the web
<a href="https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=SjVdvUPH0q" target="_blank" >https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=SjVdvUPH0q</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1016/j.micromeso.2025.113514" target="_blank" >10.1016/j.micromeso.2025.113514</a>
Alternative languages
Result language
angličtina
Original language name
Shedding electrons on ADOR zeolite structures – Structure determination by 3DED
Original language description
Three-dimensional electron diffraction (3DED) offers a powerful alternative to single-crystal X-ray diffraction (SCXRD) for the structure determination of crystalline materials with small-sized crystals (usually nanometresized) or crystals with intergrowths, often produced during zeolite synthesis. ADOR is a synthesis strategy of novel daughter zeolites from well-known parent germanosilicates. Structure determination of such ADOR zeolites is challenging due to the presence of aggregated intergrowths, and often small-sized crystals. This work demonstrates the application of continuous rotation electron diffraction (cRED), a type of 3DED, for the rapid structural characterisation of zeolites produced by ADOR approach. cRED can be performed in a transmission electron microscope and the structure of a studied material can be obtained rapidly. We propose a unified workflow for the structure determination of ADOR daughter materials. This workflow involves the initial structural investigation and determination of the parent material, followed by the utilization of this knowledge to facilitate the subsequent structure determination of the daughter material. Investigation strategy was shown to be uniform, as presented for ADOR transformation of two different parent germanosilicates. This approach is a tool allowing prompt recognition of new ADOR zeolites at the early stage of their synthesis and can be used for a feedback-based optimisation of synthesis conditions.
Czech name
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Czech description
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Classification
Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10403 - Physical chemistry
Result continuities
Project
Result was created during the realization of more than one project. More information in the Projects tab.
Continuities
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)
Others
Publication year
2025
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Microporous and Mesoporous Materials
ISSN
1387-1811
e-ISSN
1873-3093
Volume of the periodical
387
Issue of the periodical within the volume
April
Country of publishing house
NL - THE KINGDOM OF THE NETHERLANDS
Number of pages
10
Pages from-to
113514
UT code for WoS article
001412693600001
EID of the result in the Scopus database
2-s2.0-85216094955