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Isolation of Quaternary Benzo[c] phenanthridine Alkaloids from Macleaya microcarpa (MAXIM.) FEDDE: Comparison of Maceration, Soxhlet Extraction and Pressurised Liquid Extraction

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14110%2F12%3A00057370" target="_blank" >RIV/00216224:14110/12:00057370 - isvavai.cz</a>

  • Result on the web

    <a href="http://dx.doi.org/10.1002/pca.2344" target="_blank" >http://dx.doi.org/10.1002/pca.2344</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/pca.2344" target="_blank" >10.1002/pca.2344</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Isolation of Quaternary Benzo[c] phenanthridine Alkaloids from Macleaya microcarpa (MAXIM.) FEDDE: Comparison of Maceration, Soxhlet Extraction and Pressurised Liquid Extraction

  • Original language description

    Macleaya microcarpa (Papaveraceae family) has been of considerable interest in recent years as a prospective source of quaternary benzo[c]phenanthridine alkaloids (QBAs) related to many pharmaceutical beneficial effects. For this purpose, a quantitative,efficient and fast method to isolate the QBAs from the plant material is required. To optimise and compare pressurised liquid extraction (PLE) with Soxhlet extraction and maceration in order to estimate extraction conditions for fast and efficient isolation of QBAs contained in the roots of Macleaya microcarpa. The QBAs were extracted by PLE, Soxhlet extraction and maceration at different conditions (solvent, time, etc.). Reversed phase HPLC with diode-array detector was utilised for their determination and quantification. To optimise the PLE procedure, the variable parameters, including temperature (40C-150C), sample-to-inert material ratio, extraction time (5-30 min) and number of extraction cycles (1-4), were also tested.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CE - Biochemistry

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GA525%2F08%2F0819" target="_blank" >GA525/08/0819: Plant sources of minor benzophenanthridine alkaloids and study of their interaction with DNA</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>S - Specificky vyzkum na vysokych skolach

Others

  • Publication year

    2012

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Phytochemical Analysis

  • ISSN

    0958-0344

  • e-ISSN

  • Volume of the periodical

    23

  • Issue of the periodical within the volume

    5

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    6

  • Pages from-to

    477-482

  • UT code for WoS article

    000307546500009

  • EID of the result in the Scopus database