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Monitoring of Dithiothreitol Clearance by Micellar Electrokinetic Chromatography

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14310%2F01%3A00004409" target="_blank" >RIV/00216224:14310/01:00004409 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Monitoring of Dithiothreitol Clearance by Micellar Electrokinetic Chromatography

  • Original language description

    Dithiothreitol (DTT) is a well known sulfhydryl reagent used to protect the sulfhydryl groups of small molecular compounds and proteins in a variety of biochemical applications. The radioprotective action of the compound has received significant attention for a number of years. Recently DTT has been applied in studies on heat cell killing as a result of interest in hyperthermia as a cancer treatment modality. DTT is also routinely used to solubilize recombinant proteins from inclusion bodies. Previous methods used to determine DTT in solutions have included spectrophotometry and HPLC with UV spectrophotometric and fluorescence detection. We proposed the application of the on-column reaction of DTT with the reactive disulphide - 2,2-dipyridyldisulphide(DPDS) for monitoring of DTT clearance. DPDS and a sample of DTT are injected consecutively in the capillary as two discrete plugs separated with short plug of background electrolyte. Due to the differences in the mobilities of the DPDS a

  • Czech name

  • Czech description

Classification

  • Type

    D - Article in proceedings

  • CEP classification

    CE - Biochemistry

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GA525%2F00%2F0785" target="_blank" >GA525/00/0785: Acidification processes in sulphide wastes</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2001

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Article name in the collection

    Book of abstract 2nd International symposium "Separations in BioSciences SBS 2001"

  • ISBN

    80-7080-437-8

  • ISSN

  • e-ISSN

  • Number of pages

    1

  • Pages from-to

    86

  • Publisher name

    Czech Chemical Society

  • Place of publication

    Prague

  • Event location

    Prague

  • Event date

    Jan 1, 2001

  • Type of event by nationality

    WRD - Celosvětová akce

  • UT code for WoS article