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LASER ABLATION INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY - TOOL FOR ELEMENTAL MAPPING

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14310%2F09%3A00029843" target="_blank" >RIV/00216224:14310/09:00029843 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    LASER ABLATION INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY - TOOL FOR ELEMENTAL MAPPING

  • Original language description

    Laser ablation (LA) can be used as a local-sampling method for inductively coupled plasma mass spectrometry (ICP-MS). This connection allows multielemental mapping with high lateral resolution. Utilization of LA-ICP-MS for lateral elemental mapping of corroded layers is reported in this work. Molten fluoride salts (LiF-NaF) are examined as a cooling media for molten salt and high temperature reactors, nowadays. Molten fluoride salts represent a considerably invasive and corrosive media for the materialof piping and other circuit parts. Structural materials of heat exchangers may be attacked at temperatures of about 700 C and the melt-alloy interaction provokes microstructure and composition changes of contact surface. Resulting corroded layers was studied by means of LA-ICP-MS. Laser spot size of 12 mikrons was used for lateral mapping. For quantification purposes was used a sum normalization calibration procedure.

  • Czech name

  • Czech description

Classification

  • Type

    O - Miscellaneous

  • CEP classification

    CB - Analytical chemistry, separation

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GA101%2F08%2F1100" target="_blank" >GA101/08/1100: Study of interactions of cooling media at high temperatures with structural materials of heat exchangers by plasma spectrometry methods</a><br>

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2009

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů