Extraction and determination of trinitrotoluenes and produkt of their biotransformation in soil samples.
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14310%2F09%3A00039244" target="_blank" >RIV/00216224:14310/09:00039244 - isvavai.cz</a>
Result on the web
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DOI - Digital Object Identifier
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Alternative languages
Result language
angličtina
Original language name
Extraction and determination of trinitrotoluenes and produkt of their biotransformation in soil samples.
Original language description
The separation of a mixture of trinitrotoluenes (TNTs) and their metabolites by reverse phase liquid chromatography using different columns with octadecyl stationary phase is presented. The retention behaviour of a mixture of TNTs and 15 their metabolites was studied under different chromatographic conditions. The mixture of methanol/water was used as a mobile phase in isocratic and gradient modes. The effect of content of organic modifier and temperature of mobile phase has been investigated. Very goodRP-HPLC separation of 14 nitroaromatic compounds was obtained using stepped gradient elution. Different properties of 20 extraction procedures for isolation of trinitrotoluenes and their metabolites from soil were tested. Experimental conditions of Soxhlet warm extraction (extractant type, extraction time) suitable for efficient extraction of individual analytes were studied.
Czech name
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Czech description
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Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CB - Analytical chemistry, separation
OECD FORD branch
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Result continuities
Project
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Continuities
Z - Vyzkumny zamer (s odkazem do CEZ)
Others
Publication year
2009
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
International Journal of environmental analytical Chemistry
ISSN
0306-7319
e-ISSN
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Volume of the periodical
89/2009
Issue of the periodical within the volume
8-12
Country of publishing house
GB - UNITED KINGDOM
Number of pages
12
Pages from-to
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UT code for WoS article
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EID of the result in the Scopus database
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