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Laser ablation Methods for Analysis of Urinary Stones: Comparison Study Based on Calibration Pellets

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14740%2F12%3A00061405" target="_blank" >RIV/00216224:14740/12:00061405 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216305:26210/12:PU101656

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Laser ablation Methods for Analysis of Urinary Stones: Comparison Study Based on Calibration Pellets

  • Original language description

    Methods based on laser ablation, such as Laser Induced Breakdown Spectroscopy (LIBS) and Laser Ablation Inductively Coupled Plasma Mass/Optical Emission Spectrometry (LA-ICP-MS/OES) are particularly suitable for urinary stones bulk and micro analysis. The aim of this study is to demonstrate the calibration capabilities and limitations of these techniques. There are no commercially available standards, which would correspond to urinary calculi matrix. Internal standardization is also difficult, mainly due to different crystalline phases in one kidney stone. Calibration pellets were prepared from human urinary stones with phosphate, oxalate and urate matrix. For this comparative study the most frequently used laser-ablation based analytical techniques were chosen, such as LIBS and LA-ICP-MS. Moreover some unconventional techniques such as simultaneous LIBS ? LA-ICP-OES and laser ablation (LA) ? LIBS were also utilized.

  • Czech name

  • Czech description

Classification

  • Type

    O - Miscellaneous

  • CEP classification

    CB - Analytical chemistry, separation

  • OECD FORD branch

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2012

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů