Synthesis of esters derived from 2,3,4,6-tetra-O-acetyl-1-[4-(2-hydroxyethyl)-1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose

Result code in IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F13%3A39896179" target="_blank" >RIV/00216275:25310/13:39896179 - isvavai.cz</a>

Result on the web

<a href="http://dx.doi.org/10.5155/eurjchem.4.1.64-69.735" target="_blank" >http://dx.doi.org/10.5155/eurjchem.4.1.64-69.735</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.5155/eurjchem.4.1.64-69.735" target="_blank" >10.5155/eurjchem.4.1.64-69.735</a>

Result language

angličtina

Original language name

Synthesis of esters derived from 2,3,4,6-tetra-O-acetyl-1-[4-(2-hydroxyethyl)-1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose

Original language description

2,3,4,6-Tetra-O-acetyl-1-[4-(2-hydroxyethyl)- 1H-1,2,3-triazol-1-yl]-beta-D-glucopyranose was prepared and reacted with several acids, either commercially available or prepared. These included, aliphatic or aromatic acids (phenylacetic acid derivatives,benzoic derivatives), palmitic acid and the protected amino acids N-(benzyloxycarbonyl)glycine and N-(tert- butyloxycarbonyl)phenylalanine. Two other acids, 2-(3-bromopropoxy)benzoic acid and 2- (5-bromopentoxy)benzoic acid (analogues of salicylic acid were synthesized), whose preparation is also described in this work. The esterification was performed either with N,N'- dicyclohexylcarbodiimide (DCC)/4-dimethylaminopyridine (DMAP) or by reacting the acyl chlorides with the alcohol in the presence of triethylamine. The products were isolated in fair yields and fully characterized by the usual analytical techniques.

Czech name

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Czech description

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Type

J_x - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

CEP classification

CC - Organic chemistry

OECD FORD branch

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Project

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Continuities

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Publication year

2013

Confidentiality

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical

European Journal of Chemistry

ISSN

2153-2249

e-ISSN

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Volume of the periodical

4

Issue of the periodical within the volume

1

Country of publishing house

US - UNITED STATES

Number of pages

6

Pages from-to

64-69

UT code for WoS article

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EID of the result in the Scopus database

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