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Synthesis of 2,2-dinitroethene-1,1-diamine from 2 methylpyrimidine-4,6-diol and treatment of the dinitromethane produced

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F18%3A39912887" target="_blank" >RIV/00216275:25310/18:39912887 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Synthesis of 2,2-dinitroethene-1,1-diamine from 2 methylpyrimidine-4,6-diol and treatment of the dinitromethane produced

  • Original language description

    2,2-Dinitroethene-1,1-diamine (FOX-7) was prepared from 2-methylpyrimidine-4,6-diol. Dinitromethane remaining in the spent acid was disposed of by thermal decomposition or reduction with iron. Dinitromethane content in reaction mixtures was monitored by FTIR, UV-Vis spectroscopy and thin layer chromatography (TLC). Possible reuse of dinitrome¬thane is discussed. The thermal decomposition of the spent acid was studied using accelerating rate calorimetry (ARC).

  • Czech name

  • Czech description

Classification

  • Type

    D - Article in proceedings

  • CEP classification

  • OECD FORD branch

    10401 - Organic chemistry

Result continuities

  • Project

    <a href="/en/project/FV10332" target="_blank" >FV10332: Advanced chemical gas generators, not only for the automotive industry.</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2018

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Article name in the collection

    Proceedings of the 21st Seminar on New Trends in Research of Energetic Materials

  • ISBN

    978-80-7560-136-0

  • ISSN

  • e-ISSN

    neuvedeno

  • Number of pages

    10

  • Pages from-to

    703-712

  • Publisher name

    Univerzita Pardubice

  • Place of publication

    Pardubice

  • Event location

    Pardubice

  • Event date

    Apr 18, 2018

  • Type of event by nationality

    WRD - Celosvětová akce

  • UT code for WoS article