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Tuning the CHA framework composition by isomorphous substitution for CO2/CH4 separation

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F22%3A39919510" target="_blank" >RIV/00216275:25310/22:39919510 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216208:11310/22:10436161

  • Result on the web

    <a href="https://www.sciencedirect.com/science/article/pii/S1385894721028588?via%3Dihub" target="_blank" >https://www.sciencedirect.com/science/article/pii/S1385894721028588?via%3Dihub</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.cej.2021.131277" target="_blank" >10.1016/j.cej.2021.131277</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Tuning the CHA framework composition by isomorphous substitution for CO2/CH4 separation

  • Original language description

    Chemically and structurally flexible zeolites that adapt to coordinate extra-framework cations show a rich variety of gas adsorption behavior. Zeolite framework composition can be tuned to optimize pore geometry and host-guest interaction to improve selectivity. Herein, we report the study on the influence of zeolite framework nature on the separation of CO2/CH4, for CHA system containing variable isomorphously substituted heteroelements (none, B, Al, Ga, and Ti). Their performance has been evaluated by single-component isotherms and the overall separation ability was found to be related to both the geometry of 8-ring pore apertures in CHA and interaction between zeolite host and guest molecules, as revealed by Rietveld refinement of PXRD after dehydration and variable-pressure FTIR spectroscopy. Nearly isotropic geometry of the 8-ring pore opening in Al-CHA (3.84 x 3.89 angstrom) was obtained, while Ga-CHA exhibits the largest distortion (3.76 x 3.93 angstrom). Despite the smallest ionic radius of B, both the pore size of 8-ring (3.76 x 3.86 angstrom) as well as the unit cell volume are the smallest amongst the studied materials. Due to the combination of both the textural and the chemical factors, the maximum CO2 capacity and separation selectivity over CH4 follows the order Al-CHA &gt; Ga-CHA &gt; B-CHA approximate to Si-CHA &gt; Ti-CHA. These observations suggest that tuning the framework composition of zeolite can strongly influence the separation of small molecules such as CO2 and CH4.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    20401 - Chemical engineering (plants, products)

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2022

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Chemical Engineering Journal

  • ISSN

    1385-8947

  • e-ISSN

    1873-3212

  • Volume of the periodical

    429

  • Issue of the periodical within the volume

    February

  • Country of publishing house

    CH - SWITZERLAND

  • Number of pages

    8

  • Pages from-to

    "131277-1"-"131277-8"

  • UT code for WoS article

    000728573800002

  • EID of the result in the Scopus database

    2-s2.0-85115657132