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Atomic layer deposited Ir nanostructures on titania nanotube layers for efficient alkaline hydrogen evolution reaction

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F25%3A39923245" target="_blank" >RIV/00216275:25310/25:39923245 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216305:26620/26:0198250

  • Result on the web

    <a href="https://www.sciencedirect.com/science/article/pii/S0013468625009685?via%3Dihub" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0013468625009685?via%3Dihub</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.electacta.2025.146607" target="_blank" >10.1016/j.electacta.2025.146607</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Atomic layer deposited Ir nanostructures on titania nanotube layers for efficient alkaline hydrogen evolution reaction

  • Original language description

    Herein, we present the deposition and use of Iridium (Ir) electrocatalysts by Atomic Layer Deposition (ALD) on TiO2 nanotube layers (TNTs) towards Hydrogen Evolution Reaction (HER) in alkaline media. We demonstrate a precise control over Ir ALD deposition by varying the number of ALD cycles from 25 to 300, obtaining singleatoms (SAs), clusters and nanoparticles (NPs). TNTs decorated with Ir using 200 ALD cycles exhibited superior HER performance with a low overpotential value of 34 mV, minimal charge transfer resistance of 0.2 Omega and a low Tafel slope of 37 mV dec-1. Long-term stability tests revealed gradual activity degradation due to a partial oxidation of Ir. Notably, while the 200 cycles coating showed the lowest overpotential, the 150 cycles coating demonstrated the highest turnover frequency (TOF) of 1.08 s-1, indicating that optimal use of the available active sites for improved HER performance. This results from the balance between the Ir content and the available active sites, rather than solely relying on electrochemically active surface area (ECSA) or overpotential values. This work provides insights into the complex relationship between Ir nanostructure, oxidation states and catalytic efficiency, contributing to the development of more effective HER catalysts.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10405 - Electrochemistry (dry cells, batteries, fuel cells, corrosion metals, electrolysis)

Result continuities

  • Project

    <a href="/en/project/GX23-08019X" target="_blank" >GX23-08019X: Single-Atom-based 2D-Photocatalysts</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2025

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Electrochimica Acta

  • ISSN

    0013-4686

  • e-ISSN

    1873-3859

  • Volume of the periodical

    535

  • Issue of the periodical within the volume

    September 2025

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    9

  • Pages from-to

    146607

  • UT code for WoS article

    001506292100007

  • EID of the result in the Scopus database

    2-s2.0-105007143159