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Comparison of laser diffractometry and pipetting methods for particle size determination: A pilot study on the implications of result discrepancies on soil classification

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26110%2F24%3APU154991" target="_blank" >RIV/00216305:26110/24:PU154991 - isvavai.cz</a>

  • Result on the web

    <a href="https://acsess.onlinelibrary.wiley.com/doi/epdf/10.1002/saj2.20791" target="_blank" >https://acsess.onlinelibrary.wiley.com/doi/epdf/10.1002/saj2.20791</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/saj2.20791" target="_blank" >10.1002/saj2.20791</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Comparison of laser diffractometry and pipetting methods for particle size determination: A pilot study on the implications of result discrepancies on soil classification

  • Original language description

    In recent decades, the determination of particle size distribution (PSD) using the laser diffraction method (LDM) has become increasingly common, supplanting traditional sedimentation techniques. Advances in everything from sample preparation to software settings have been realized globally, whether through recommendations from laser diffraction (LD) manufacturers or through user experiences. These developments seek to enhance accuracy and diminish the uncertainties associated with new methodologies. Particularly in the determination of PSD using LDM on various LD instruments and in comparison with the sieve-pipette method (SPM), discrepancies in PSD frequently arise. This article aims to mitigate these discrepancies by predefining parameters, specifically through the adjustment of LD software settings and sample preparation (employing a uniform set of dispersed samples in potassium hydroxide) on two widely used LD instruments for soil measurements: Mastersizer 3000 and Analysette 22. Additionally, these samples were analyzed using the traditional SPM (ISO 11277, 1998), with the results from LDM and SPM subsequently compared. The paper also explores the impact, range of user options, and limitations of predefined software settings on both LD instruments. Eighty soil samples were analyzed for PSD, collected from arable land in the cadastral area of Hru & scaron;ky, district of B & rcaron;eclav (Czech Republic), in spring 2022, from depths of 0- to 10-cm and 10- to 20-cm. Significant differences in PSD were confirmed, although the trends of the grain size distribution curves were very similar to those of LDM. Results from the Mastersizer underestimated the clay fraction by an average of 17% compared to SPM, at the expense of the sand fraction, whereas the silt fraction was underestimated by a maximum of 4%. Conversely, Analysette 22 overestimated the silt fraction by an average of 37% at the expense of the sand fraction, confirming only a slight difference in the clay

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    40104 - Soil science

Result continuities

  • Project

  • Continuities

    S - Specificky vyzkum na vysokych skolach

Others

  • Publication year

    2024

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    SOIL SCIENCE SOCIETY OF AMERICA JOURNAL

  • ISSN

    0361-5995

  • e-ISSN

    1435-0661

  • Volume of the periodical

    89

  • Issue of the periodical within the volume

    1

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    16

  • Pages from-to

    „“-„“

  • UT code for WoS article

    001377183600001

  • EID of the result in the Scopus database