Application of Low-temperature Low-pressure Hydrogen Plasma: Treatment of Artificially Prepared Corrosion Layers

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26310%2F15%3APU110475" target="_blank" >RIV/00216305:26310/15:PU110475 - isvavai.cz</a>
Result on the web
<a href="https://www.degruyter.com/view/journals/chem/open-issue/article-10.1515-chem-2015-0045/article-10.1515-chem-2015-0045.xml" target="_blank" >https://www.degruyter.com/view/journals/chem/open-issue/article-10.1515-chem-2015-0045/article-10.1515-chem-2015-0045.xml</a>
DOI - Digital Object Identifier
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Result language
angličtina
Original language name
Application of Low-temperature Low-pressure Hydrogen Plasma: Treatment of Artificially Prepared Corrosion Layers
Original language description
The aim of this work is the application of low-temperature low-pressure hydrogen plasma on artificially prepared corrosion layers, so called plasma chemical reduction. It is necessary to use samples with artificially prepared corrosion layers because it is impossible to use the real artifacts for fundamental research. The bronze was chosen as a sample material. Formation of corrosion layers on the bronze samples was carried out in concentrated hydrochloric acid vapors with the addition of sand. The radio-frequency hydrogen plasma was generated in the flowing regime at pressure of 160 Pa. Different values of supplied power were chosen as well as different discharge modes: the continuous or the pulsed mode with varied duty cycles. By the combination of supplied power and mode factors, we selected two values of effective power. The process of plasma chemical reduction was monitored by optical emission spectroscopy (OES) and simultaneously, the sample temperature was measured. Rotational temperatures were calculated from OH radicals spectra. Changes in the structure and elemental composition were determined using scanning electron microscopy (SEM) and energy dispersive X-ray analysis (EDX).
Czech name
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Czech description
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Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10403 - Physical chemistry

Project
<a href="/en/project/DF11P01OVV004" target="_blank" >DF11P01OVV004: Plasma chemical processes and technologies for conservation of archaeological metallic objects</a><br>
Continuities
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Publication year
2015
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

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