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The effect of aminooxy-linkers' structure on the mechanical properties of hyaluronan-oxime hydrogels

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26310%2F22%3APU147695" target="_blank" >RIV/00216305:26310/22:PU147695 - isvavai.cz</a>

  • Result on the web

    <a href="https://web-p-ebscohost-com.ezproxy.lib.vutbr.cz/ehost/pdfviewer/pdfviewer?vid=0&sid=8dd8c0ea-6e22-44c5-b745-c30352736dd8%40redis" target="_blank" >https://web-p-ebscohost-com.ezproxy.lib.vutbr.cz/ehost/pdfviewer/pdfviewer?vid=0&sid=8dd8c0ea-6e22-44c5-b745-c30352736dd8%40redis</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.3144/expresspolymlett.2022.21" target="_blank" >10.3144/expresspolymlett.2022.21</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    The effect of aminooxy-linkers' structure on the mechanical properties of hyaluronan-oxime hydrogels

  • Original language description

    The wide range of hydrogel applications is a result of the optimization of gelation. Herein, the various aminooxylinkers were synthesized to study the kinetics of gelation and mechanical properties of hydrogels prepared by crosslinking of aldehyde-modified N-acetylglucosamine (GlcNAc) of hyaluronan (Delta HA-CHO: 4,5-anhydro-6-(GlcNAc)-oxo hyaluronan or HA-CHO: 6-(GlcNAc)-oxo hyaluronan). Structural characteristics of the linkers (length, number of functional groups and rigidity) and the polymer (effect of the -C=C- double bond) were investigated in detail and showed decreasing mechanical stiffness with increasing hydrophobic character of linker and effect of its rigidity/flexibility on imine conversion. Besides known linear bis(aminooxy)alkanes with different lengths of the chain, new multifunctional aminooxy-linkers: 1,3,5tris(aminooxymethyl)benzene and multikis(6-aminooxy-6-deoxy)-beta-cyclodextrin were prepared and shortened the gelation time. The MTT (3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide) analysis showed that despite the aminooxylinkers ' cytotoxicity at higher concentrations, the final oxime hydrogels are non-cytotoxic and therefore are suitable for medicinal applications.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10400 - Chemical sciences

Result continuities

  • Project

  • Continuities

    S - Specificky vyzkum na vysokych skolach

Others

  • Publication year

    2022

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    EXPRESS POLYM LETT

  • ISSN

    1788-618X

  • e-ISSN

  • Volume of the periodical

    16

  • Issue of the periodical within the volume

    3

  • Country of publishing house

    HU - HUNGARY

  • Number of pages

    14

  • Pages from-to

    265-278

  • UT code for WoS article

    000752462200005

  • EID of the result in the Scopus database

    2-s2.0-85125920148