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Itaconic anhydride homopolymerization during radical grafting of poly(lactic acid) in melt

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26620%2F17%3APU124183" target="_blank" >RIV/00216305:26620/17:PU124183 - isvavai.cz</a>

  • Result on the web

    <a href="http://www.sciencedirect.com/science/article/pii/S1381514817300950" target="_blank" >http://www.sciencedirect.com/science/article/pii/S1381514817300950</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.reactfunctpolym.2017.05.004" target="_blank" >10.1016/j.reactfunctpolym.2017.05.004</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Itaconic anhydride homopolymerization during radical grafting of poly(lactic acid) in melt

  • Original language description

    This is the first study that focused on the homopolymerization of itaconic anhydride (IAH) during melt radical grafting of poly(lactic acid) (PLA) at 190 °C. Although neglected by many authors, in the present study, radical- induced IAH homopolymerization, self-induced IAH homopolymerization, and IAH isomerization to citraconic anhydride were studied. The yield of investigated IAH-based side reactions was determined by Fourier transform infrared spectroscopy, and reaction by-products were extracted from raw PLA-g-IAH and characterized by thermogravimetric analysis (TGA) and size exclusion chromatography (SEC). It was found that the highest concentration of IAH and L101 favors IAH homopolymerization and affects the PLA grafting reaction mechanism dramatically.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10404 - Polymer science

Result continuities

  • Project

    <a href="/en/project/LQ1601" target="_blank" >LQ1601: CEITEC 2020</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2017

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    REACTIVE & FUNCTIONAL POLYMERS

  • ISSN

    1381-5148

  • e-ISSN

    1873-166X

  • Volume of the periodical

    neuveden

  • Issue of the periodical within the volume

    116

  • Country of publishing house

    NL - THE KINGDOM OF THE NETHERLANDS

  • Number of pages

    8

  • Pages from-to

    49-56

  • UT code for WoS article

    000403519800007

  • EID of the result in the Scopus database

    2-s2.0-85019441660