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Catalyst Formation and In Operando Monitoring of the Electrocatalytic Activity in Flow Reactors

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26620%2F21%3APU141637" target="_blank" >RIV/00216305:26620/21:PU141637 - isvavai.cz</a>

  • Alternative codes found

    RIV/62156489:43210/21:43920254

  • Result on the web

    <a href="https://pubs.acs.org/doi/10.1021/acsami.1c09127" target="_blank" >https://pubs.acs.org/doi/10.1021/acsami.1c09127</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1021/acsami.1c09127" target="_blank" >10.1021/acsami.1c09127</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Catalyst Formation and In Operando Monitoring of the Electrocatalytic Activity in Flow Reactors

  • Original language description

    Flow reactors are of increasing importance and have become crucial devices due to their wide application in chemical synthesis, electrochemical hydrogen evolution reaction (HER), or electrochemical waste water treatment. In many of these applications, catalyst materials such as transition-metal chalcogenides (TMCs) for the HER, provide the desired electrochemical reactivity for the HER. Generally, the flow electrolyzers' performance is evaluated as the overall output, but the decrease in activity of the electrolyzer is due to localized failure of the catalyst. Herein, we present a method for the spatially resolved (tens of micrometers) In Operando analysis of the catalytic activity under real operation conditions as well as the localized deposition of the catalyst in an operating model flow reactor. For these purposes, scanning electrochemical microscopy was applied for MoSx catalyst deposition and for localized tracking of the TMC activity with a resolution of 25 mu m. This approach offers detailed information about the catalytic performance and should find broad application for the characterization and optimization of flow reactor catalysis under real operational conditions.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    21001 - Nano-materials (production and properties)

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2021

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    ACS APPL MATER INTER

  • ISSN

    1944-8244

  • e-ISSN

    1944-8252

  • Volume of the periodical

    13

  • Issue of the periodical within the volume

    30

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    8

  • Pages from-to

    35777-35784

  • UT code for WoS article

    000683741400049

  • EID of the result in the Scopus database

    2-s2.0-85111575858