Pressure assisted sintering of Al2O3-Y2O3 glass microspheres: sintering conditions, grain size, and mechanical properties of sintered ceramics

Result code in IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26620%2F22%3APU143954" target="_blank" >RIV/00216305:26620/22:PU143954 - isvavai.cz</a>

Result on the web

<a href="https://www.degruyter.com/document/doi/10.1515/pac-2021-0705/html" target="_blank" >https://www.degruyter.com/document/doi/10.1515/pac-2021-0705/html</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1515/pac-2021-0705" target="_blank" >10.1515/pac-2021-0705</a>

Result language

angličtina

Original language name

Pressure assisted sintering of Al2O3-Y2O3 glass microspheres: sintering conditions, grain size, and mechanical properties of sintered ceramics

Original language description

Glass microspheres with yttria-alumina eutectic composition (76.8 mol % Al2O3 and 23.2 mol % Y2O3) were prepared by sol-gel Pechini method and flame synthesis with or without subsequent milling. Prepared amorphous powders were studied by X-ray powder diffraction (XRD), particle size analysis (PSA), scanning electron microscopy (SEM) and differential thermal analysis (DTA). Hot pressing (HP), rapid hot pressing (RHP) and spark plasma sintering (SPS) were used to sinter amorphous precursor powders at 1600 degrees C without holding time (0 min). The preparation process including milling step resulted in amorphous powders with narrower particle size distribution and smaller particle size. All applied pressure assisted sintering techniques resulted in dense bulk samples with fine grained microstructure consisting of irregular alpha-Al2O3 and Y3Al5O12 (YAG) grains. Milling was beneficial in terms of final microstructure refinement and mechanical properties of sintered materials. A material with the Vickers hardness of HV = (17.1 +/- 0.3) GPa and indentation fracture resistance of (4.2 +/- 0.2) MPa.m(1/2) was prepared from the powder milled for 12 h.

Czech name

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Czech description

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Type

J_imp - Article in a specialist periodical, which is included in the Web of Science database

CEP classification

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OECD FORD branch

10403 - Physical chemistry

Project

—

Continuities

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Publication year

2022

Confidentiality

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical

PURE AND APPLIED CHEMISTRY

ISSN

0033-4545

e-ISSN

1365-3075

Volume of the periodical

94

Issue of the periodical within the volume

2

Country of publishing house

GB - UNITED KINGDOM

Number of pages

11

Pages from-to

157-167

UT code for WoS article

000739605800001

EID of the result in the Scopus database

2-s2.0-85120814279