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Intrinsic properties of anodic TiO2 nanotube layers: In-situ XRD annealing of TiO2 nanotube layers

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26620%2F23%3APU147475" target="_blank" >RIV/00216305:26620/23:PU147475 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216275:25310/23:39920472

  • Result on the web

    <a href="https://www.sciencedirect.com/science/article/pii/S0272884222039992?via%3Dihub" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0272884222039992?via%3Dihub</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.ceramint.2022.11.032" target="_blank" >10.1016/j.ceramint.2022.11.032</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Intrinsic properties of anodic TiO2 nanotube layers: In-situ XRD annealing of TiO2 nanotube layers

  • Original language description

    In this work, in-situ annealing of TiO2 nanotube (TNT) layers in an XRD chamber was carried out to investigate the crystallization process of the TNT layers in details. TNT layers of different thicknesses, i.e. 1, 5 and 20 μm, and of different morphology, i.e. double wall vs. single wall, were annealed in the temperature range from room temperature to 500 °C with two distinctly different annealing rates. Additionally, three different annealing atmospheres were explored, namely air as an oxidative, N2 as an inert, and 5%H2/95%N2 as a reductive atmosphere. XRD patterns were measured every 15 °C of the heating ramp and the crystallite sizes of anatase phase were calculated from the anatase peak using Scherer equation at each data point. The differences in crystallization behavior for the different TNT layers as well as the effect of the annealing atmosphere for 5 μm thick TNT layers are described and discussed.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10405 - Electrochemistry (dry cells, batteries, fuel cells, corrosion metals, electrolysis)

Result continuities

  • Project

  • Continuities

Others

  • Publication year

    2023

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Ceramics International

  • ISSN

    0272-8842

  • e-ISSN

    1873-3956

  • Volume of the periodical

    49

  • Issue of the periodical within the volume

    14

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    9

  • Pages from-to

    24293-24301

  • UT code for WoS article

    001017504900001

  • EID of the result in the Scopus database

    2-s2.0-85141959203