Intrinsic properties of anodic TiO2 nanotube layers: In-situ XRD annealing of TiO2 nanotube layers
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26620%2F23%3APU147475" target="_blank" >RIV/00216305:26620/23:PU147475 - isvavai.cz</a>
Alternative codes found
RIV/00216275:25310/23:39920472
Result on the web
<a href="https://www.sciencedirect.com/science/article/pii/S0272884222039992?via%3Dihub" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0272884222039992?via%3Dihub</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1016/j.ceramint.2022.11.032" target="_blank" >10.1016/j.ceramint.2022.11.032</a>
Alternative languages
Result language
angličtina
Original language name
Intrinsic properties of anodic TiO2 nanotube layers: In-situ XRD annealing of TiO2 nanotube layers
Original language description
In this work, in-situ annealing of TiO2 nanotube (TNT) layers in an XRD chamber was carried out to investigate the crystallization process of the TNT layers in details. TNT layers of different thicknesses, i.e. 1, 5 and 20 μm, and of different morphology, i.e. double wall vs. single wall, were annealed in the temperature range from room temperature to 500 °C with two distinctly different annealing rates. Additionally, three different annealing atmospheres were explored, namely air as an oxidative, N2 as an inert, and 5%H2/95%N2 as a reductive atmosphere. XRD patterns were measured every 15 °C of the heating ramp and the crystallite sizes of anatase phase were calculated from the anatase peak using Scherer equation at each data point. The differences in crystallization behavior for the different TNT layers as well as the effect of the annealing atmosphere for 5 μm thick TNT layers are described and discussed.
Czech name
—
Czech description
—
Classification
Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
—
OECD FORD branch
10405 - Electrochemistry (dry cells, batteries, fuel cells, corrosion metals, electrolysis)
Result continuities
Project
—
Continuities
—
Others
Publication year
2023
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Ceramics International
ISSN
0272-8842
e-ISSN
1873-3956
Volume of the periodical
49
Issue of the periodical within the volume
14
Country of publishing house
GB - UNITED KINGDOM
Number of pages
9
Pages from-to
24293-24301
UT code for WoS article
001017504900001
EID of the result in the Scopus database
2-s2.0-85141959203