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The Dispersion-Strengthening Effect of TiN Nanoparticles Evoked by Ex Situ Nitridation of Gas-Atomized, NiCu-Based Alloy 400 in Fluidized Bed Reactor for Laser Powder Bed Fusion

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26620%2F24%3APU152632" target="_blank" >RIV/00216305:26620/24:PU152632 - isvavai.cz</a>

  • Result on the web

    <a href="https://www.mdpi.com/2504-4494/8/5/223" target="_blank" >https://www.mdpi.com/2504-4494/8/5/223</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.3390/jmmp8050223" target="_blank" >10.3390/jmmp8050223</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    The Dispersion-Strengthening Effect of TiN Nanoparticles Evoked by Ex Situ Nitridation of Gas-Atomized, NiCu-Based Alloy 400 in Fluidized Bed Reactor for Laser Powder Bed Fusion

  • Original language description

    Throughout recent years, the implementation of nanoparticles into the microstructure of additively manufactured (AM) parts has gained great attention in the material science community. The dispersion strengthening (DS) effect achieved leads to a substantial improvement in the mechanical properties of the alloy used. In this work, an ex situ approach of powder conditioning prior to the AM process as per a newly developed fluidized bed reactor (FBR) was applied to a titanium-enriched variant of the NiCu-based Alloy 400. Powders were investigated before and after FBR exposure, and it was found that the conditioning led to a significant increase in the TiN formation along grain boundaries. Manufactured to parts via laser-based powder bed fusion of metals (PBF-LB/M), the ex situ FBR approach not only revealed a superior microstructure compared to unconditioned parts but also with respect to a recently introduced in situ approach based on a gas atomization reaction synthesis (GARS). A substantially higher number of nanoparticles formed along cell walls and enabled an effective suppression of dislocation movement, resulting in excellent tensile, creep, and fatigue properties, even at elevated temperatures up to 750 degrees C. Such outstanding properties have never been documented for AM-processed Alloy 400, which is why the demonstrated FBR ex situ conditioning marks a promising modification route for future alloy systems.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    21100 - Other engineering and technologies

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2024

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Journal of Manufacturing and Materials Processing

  • ISSN

    2504-4494

  • e-ISSN

  • Volume of the periodical

    223

  • Issue of the periodical within the volume

    1

  • Country of publishing house

    CH - SWITZERLAND

  • Number of pages

    29

  • Pages from-to

    „“-„“

  • UT code for WoS article

    001340933400001

  • EID of the result in the Scopus database

    2-s2.0-85207683743