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Formation of Phases in Reactively Sintered TiAl3 Alloy

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F26316919%3A_____%2F20%3AN0000012" target="_blank" >RIV/26316919:_____/20:N0000012 - isvavai.cz</a>

  • Alternative codes found

    RIV/68378271:_____/20:00533533 RIV/60461373:22310/20:43921114

  • Result on the web

    <a href="https://www.mdpi.com/1420-3049/25/8/1912/htm" target="_blank" >https://www.mdpi.com/1420-3049/25/8/1912/htm</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.3390/molecules25081912" target="_blank" >10.3390/molecules25081912</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Formation of Phases in Reactively Sintered TiAl3 Alloy

  • Original language description

    This work highlights new results on the synthesis of the TiAl3 intermetallic phase using self-propagating high-temperature synthesis. This method is considered a promising sintering route for intermetallic compounds. It was found that the reactions proceed in two stages. Below the melting point of aluminum, the Ti2Al5 phase forms at 450 degrees C after long annealing times by a direct solid-state reaction between the aluminum and titanium, and is converted consequently to TiAl3. This is a completely new finding; until now, many authors have believed in the preferential formation of the TiAl3 phase. The second stage, the self-propagating strongly exothermic reaction, proceeds above the melting point of aluminum. It leads to the formation of the TiAl3 phase accompanied by Ti2Al5 and Ti3Al phases. The reaction mechanism was shown in the form of chemical equations, which were supported by calculating Gibbs energy. Reaction temperatures (T-onset, T-maximum, and T-offset) were determined after induction heating thanks to recording by an optical pyrometer. This finding provides completely new opportunities for the determination of activation energy at heating rates, in which common calorimeters are not able to detect a response or even measure. Now, the whole procedure will become accessible.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    20501 - Materials engineering

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2020

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    MOLECULES

  • ISSN

    1420-3049

  • e-ISSN

    1420-3049

  • Volume of the periodical

    25

  • Issue of the periodical within the volume

    8

  • Country of publishing house

    CH - SWITZERLAND

  • Number of pages

    13

  • Pages from-to

    nestránkováno

  • UT code for WoS article

    000534617500070

  • EID of the result in the Scopus database

    2-s2.0-85083798339