Microstructured reactor for electroorganic synthesis.

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22310%2F10%3A00022992" target="_blank" >RIV/60461373:22310/10:00022992 - isvavai.cz</a>
Result on the web
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DOI - Digital Object Identifier
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Result language
angličtina
Original language name
Microstructured reactor for electroorganic synthesis.
Original language description
In the present work a brief overview of microstructured devices, the advantages and disadvantages as well as the principles of a multiscale design approach are presented. The advantages mainly comprise uniform current density distribution, local controlof the process parameters, high single-pass conversion of the reactant and reduced concentration of the supporting electrolyte needed to perform the reaction. The main challenge with this type of cell is gas evolution, a typical reaction taking place atthe counterelectrode. The phenomena discussed are documented using the example of anodic methoxylation of 4-methylanisole. An analysis was made of the two-phase flow hydrodynamics inside the microstructured cell. The range of operational conditions suitable for the desired reaction was identified. The results were used together with the information on the electrode reaction kinetics in the form of the Butler?Volmer type equation for the design of a suitable bipolar microstructured cell.
Czech name
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Czech description
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Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CG - Electrochemistry
OECD FORD branch
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Publication year
2010
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

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