Simple synthesis of free surface nanostructured spinel NiFe2O4 with a tunable particle size
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22310%2F17%3A43913359" target="_blank" >RIV/60461373:22310/17:43913359 - isvavai.cz</a>
Alternative codes found
RIV/60461373:22340/17:43913359 RIV/60461373:22330/17:43913359
Result on the web
<a href="https://www.sciencedirect.com/science/article/pii/S0925838817321990" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0925838817321990</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1016/j.jallcom.2017.06.200" target="_blank" >10.1016/j.jallcom.2017.06.200</a>
Alternative languages
Result language
angličtina
Original language name
Simple synthesis of free surface nanostructured spinel NiFe2O4 with a tunable particle size
Original language description
Nanostructured nickel ferrite stoichiometric spinel NiFe2O4 is intensively studied as a material suitable for catalysts or medical applications. Thus, it is very important to find a simple and cost-effective method for the synthesis of nanoparticles with homogenous and tunable particle size. In this work, we successfully synthetized nickel ferrite nanoparticles by thermal decomposition of nickel-iron glycerolate in a dynamic air atmosphere at different temperatures. We studied the thermal decomposition process by STA. The nickel-iron glycerolate precursor was analyzed by XRD, XPS, AAS, Raman spectroscopy, EDS and SEM to obtain exact composition and information about the morphology. The particle size of the obtained nanoparticles was determined from XRD diffraction patterns using Scherrer equation and also by TEM. Magnetic properties were studied using VSM in PPMS.
Czech name
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Czech description
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Classification
Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10402 - Inorganic and nuclear chemistry
Result continuities
Project
<a href="/en/project/GA17-13161S" target="_blank" >GA17-13161S: The role of nonstoichimetry and nanosizing in material properties of metal oxides</a><br>
Continuities
S - Specificky vyzkum na vysokych skolach<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Others
Publication year
2017
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Journal of Alloys and Compounds
ISSN
0925-8388
e-ISSN
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Volume of the periodical
723
Issue of the periodical within the volume
NOV 5 2017
Country of publishing house
US - UNITED STATES
Number of pages
6
Pages from-to
58-63
UT code for WoS article
000407009400009
EID of the result in the Scopus database
2-s2.0-85021339260