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Mechanistic study of dissolution enhancement by interactive mixtures of chitosan with meloxicam as model

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22310%2F22%3A43925898" target="_blank" >RIV/60461373:22310/22:43925898 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216208:11160/22:10451091

  • Result on the web

    <a href="https://www.sciencedirect.com/science/article/pii/S0928098721003882?via%3Dihub" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0928098721003882?via%3Dihub</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.ejps.2021.106087" target="_blank" >10.1016/j.ejps.2021.106087</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Mechanistic study of dissolution enhancement by interactive mixtures of chitosan with meloxicam as model

  • Original language description

    To enhance dissolution rate of meloxicam (MX), a poorly soluble model drug, a natural polysaccharide excipient chitosan (CH) is employed in this work as a carrier to prepare binary interactive mixtures by either mixing or comilling techniques. The MX-CH mixtures of three different drug loads were characterized for morphological, granulometric, and thermal properties as well as drug crystallinity. The relative dissolution rate of MX was determined in phosphate buffer of pH 6.8 using the USP-4 apparatus; a significant increase in MX dissolution rate was observed for both mixed and co-milled mixtures comparing to the raw drug. Higher dissolution rate of MX was evidently connected to surface activation by mixing or milling, which was pronounced by the higher specific surface energy as detected by inverse gas chromatography. In addition to the particle size reduction, the carrier effect of the CH was confirmed for co-milling by linear regression between the MX maximum relative dissolution rate and the total surface area of the mixture (R-2 = 0.863). No MX amorphization or crystalline structure change were detected. The work of adhesion/cohesion ratio of 0.9 supports the existence of preferential adherence of MX to the coarse particles of CH to form stable interactive mixtures.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    30104 - Pharmacology and pharmacy

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2022

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    European Journal of Pharmaceutical Sciences

  • ISSN

    0928-0987

  • e-ISSN

    1879-0720

  • Volume of the periodical

    169

  • Issue of the periodical within the volume

    106087

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    12

  • Pages from-to

    nestrankovano

  • UT code for WoS article

    000804547300004

  • EID of the result in the Scopus database

    2-s2.0-85120995366