Method for analysis of 68 organic contaminants in food contact paper using gas and liquid chromatography coupled with tandem mass spectrometry

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22330%2F15%3A43899473" target="_blank" >RIV/60461373:22330/15:43899473 - isvavai.cz</a>
Alternative codes found
RIV/00216208:11310/16:10318705 RIV/75010330:_____/16:00011030
Result on the web
<a href="http://ac.els-cdn.com/S0956713515301316/1-s2.0-S0956713515301316-main.pdf?_tid=073e91c0-77f0-11e5-9c61-00000aacb362&acdnat=1445431030_6cbe344a51fe2fee4c7780c0b6ddb0f4" target="_blank" >http://ac.els-cdn.com/S0956713515301316/1-s2.0-S0956713515301316-main.pdf?_tid=073e91c0-77f0-11e5-9c61-00000aacb362&acdnat=1445431030_6cbe344a51fe2fee4c7780c0b6ddb0f4</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1016/j.foodcont.2015.07.043" target="_blank" >10.1016/j.foodcont.2015.07.043</a>

Result language
angličtina
Original language name
Method for analysis of 68 organic contaminants in food contact paper using gas and liquid chromatography coupled with tandem mass spectrometry
Original language description
Food contact materials (FCMs) have been reported as a source of various xenobiotics. This study investigates the possibility of simultaneous analysis of 68 potential contaminants in paper FCMs, specifically phthalates, polycyclic aromatic hydrocarbons, photoinitiators, bisphenols, and polyfluorinated compounds. Target compounds were co-isolated using a technique based on ultrasonic extraction by mixture of acetonitrile and water followed by QuEChERS-like liquid-liquid partition in the presence of inorganic salts. Resulting extracts were analyzed using gas and high performance liquid chromatography coupled with tandem mass spectrometry (GC-MS/MS, HPLC-MS/MS). Acceptable recoveries (70-120%) and RSDs (<20%) were achieved for most of the analytes at spiking levels of 0.05, 0.2 and 1 mg/kg. LOQs ranged from 0.0013 to 0.22 mg/kg. The proposed method was successfully applied to analysis of 15 real samples. Complex mixtures of contaminants reaching levels up to 48 mg/kg were identified in the
Czech name
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Czech description
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Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CB - Analytical chemistry, separation
OECD FORD branch
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Project
<a href="/en/project/NT14375" target="_blank" >NT14375: Identification of health hazards based on contamination from paper and cardboard foodstuff packages</a><br>
Continuities
V - Vyzkumna aktivita podporovana z jinych verejnych zdroju

Publication year
2015
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

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