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Enhancement of CO2 Affinity in a Polymer of Intrinsic Microporosity by Amine Modification

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22340%2F14%3A43896617" target="_blank" >RIV/60461373:22340/14:43896617 - isvavai.cz</a>

  • Result on the web

    <a href="http://pubs.acs.org/doi/abs/10.1021/ma401869p?prevSearch=%255BContrib%253A%2BFriess%255D&searchHistoryKey=" target="_blank" >http://pubs.acs.org/doi/abs/10.1021/ma401869p?prevSearch=%255BContrib%253A%2BFriess%255D&searchHistoryKey=</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1021/ma401869p" target="_blank" >10.1021/ma401869p</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Enhancement of CO2 Affinity in a Polymer of Intrinsic Microporosity by Amine Modification

  • Original language description

    Nitrile groups in the polymer of intrinsic microporosity PIM-1 were reduced to primary amines using borane complexes. In adsorption experiments, the novel amine?PIM-1 showed higher CO2 uptake and higher CO2/ N2 sorption selectivity than the parent polymer, with very evident dual-mode sorption behavior. In gas permeation with six light gases, the individual contributions of solubility and diffusion to the overall permeability was determined via timelag analysis. The high CO2 affinity drastically restricts diffusion at low pressures and lowers CO2 permeability compared to the parent PIM-1. Furthermore, the size-sieving properties of the polymer are increased, which can be attributed to a higher stiffness of the system arising from hydrogen bonding of theamine groups. Thus, for the H2/CO2 gas pair, whereas PIM-1 favors CO2, amine?PIM-1 shows permselectivity toward H2, breaking the Robeson 2008 upper bound.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CD - Macromolecular chemistry

  • OECD FORD branch

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2014

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Macromolecules

  • ISSN

    0024-9297

  • e-ISSN

  • Volume of the periodical

    47

  • Issue of the periodical within the volume

    3

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    9

  • Pages from-to

    1021-1029

  • UT code for WoS article

    000331344200018

  • EID of the result in the Scopus database