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Electrochemical Activity of Hydrothermally Synthesized Li-Ti-O Cubic Oxides towards Li Insertion.

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388955%3A_____%2F02%3A54020146" target="_blank" >RIV/61388955:_____/02:54020146 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Electrochemical Activity of Hydrothermally Synthesized Li-Ti-O Cubic Oxides towards Li Insertion.

  • Original language description

    Li-Ti-O oxides prepared by hydrothermal synthesis are active hosts for lithium insertion. Annealing of synthesized samples at temperatures above 250degreesC leads to structural water removal, which causes narrowing of voltammetric peaks and, subsequently, shift of the insertion potential toward more negative potentials. An increase of annealing temperature also improves coulombic efficiency and stability against self-discharge reactions. On the other hand, the lithium insertion/extraction kinetics slowsdown with increasing annealing temperature. Hydrothermally synthesized Li-Ti-O spinels show more favorable charge transfer kinetics as well lithium transport comparing with spinels prepared at 8 00degrees C. Thermodynamics of Li insertion into hydrothermally prepared phases can be described by the Frumkin insertion isotherm. The low temperature prepared spinels seem to be less susceptible to a lithium-insertion triggered phase transition than the high temperature synthesized materials.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CG - Electrochemistry

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GA203%2F99%2F0879" target="_blank" >GA203/99/0879: Electrochemical and in-situ AFM study of the electrochemical formation of oxide thin films with controlled crystallinity at elevated temperatures</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2002

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Journal of the Electrochemical Society

  • ISSN

    0013-4651

  • e-ISSN

  • Volume of the periodical

    149

  • Issue of the periodical within the volume

    9

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    6

  • Pages from-to

    1224-1229

  • UT code for WoS article

  • EID of the result in the Scopus database