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Incorporation of Aluminum and Iron into the ZSM-12 Zeolite: Synthesis and Characterization of Acid Sites.

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388955%3A_____%2F02%3A54020245" target="_blank" >RIV/61388955:_____/02:54020245 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Incorporation of Aluminum and Iron into the ZSM-12 Zeolite: Synthesis and Characterization of Acid Sites.

  • Original language description

    Zeolite ZSM-12 with aluminum and iron in the framework was synthesized in a broad range of Si/Al (Fe) ratios using methyltriethylammonium bromide as structure-directing agent with the aim to characterize the type and concentration of acid sites in dependence on Si/Al (Fe) ratios and calcination procedures. It was shown that the minimum Si/Al ratio achieved for (Al)ZSM-12 is around 35, which is very close to minimum Si/Fe ratio of about 37 for (Fe)ZSM-12. The rate of crystallization of (Al) and (Fe)ZSM-12 depends on the concentration of Al and Fe in the reaction mixture of these trivalent cations, the slower was the apparent crystallization rate. It is suggested that the crystallization rate is controlled by the number of nucleation centers, which depends on the amount of trivalent cations (Al, Fe) . Zeolites (Al) and (Fe)ZSM-12 were calcined under a variety of carefully controlled conditions to investigate the resulting concentration of Broensted and Lewis acid sites.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CF - Physical chemistry and theoretical chemistry

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/IAA4040001" target="_blank" >IAA4040001: Basic molecular sieves for selective side-chain alkylation of toluene</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2002

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Collection of Czechoslovak Chemical Commmunications

  • ISSN

    0010-0765

  • e-ISSN

  • Volume of the periodical

    67

  • Issue of the periodical within the volume

    N/A

  • Country of publishing house

    CZ - CZECH REPUBLIC

  • Number of pages

    18

  • Pages from-to

    1760-1778

  • UT code for WoS article

  • EID of the result in the Scopus database