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Fabrication of Hybrid Organic-Inorganic Materials with Tunable Porosity for Catalytic Application

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388955%3A_____%2F15%3A00446861" target="_blank" >RIV/61388955:_____/15:00446861 - isvavai.cz</a>

  • Result on the web

    <a href="http://dx.doi.org/10.1002/cplu.201402346" target="_blank" >http://dx.doi.org/10.1002/cplu.201402346</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/cplu.201402346" target="_blank" >10.1002/cplu.201402346</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Fabrication of Hybrid Organic-Inorganic Materials with Tunable Porosity for Catalytic Application

  • Original language description

    Novel layered organic-inorganic materials functionalized with amino groups have been synthesized by using a two-dimensional zeolitic precursor, IPC-1P, prepared by a top-down approach from zeolite UTL. The formation of porous materials containing silsesquioxane linkers covalently bonded to zeolite layers in the interlayer space was confirmed by a variety of characterization techniques (N(2)sorption, XRD, TEM). The textural properties and catalytic behavior of functionalized hybrid materials synthesizedby direct pillaring of IPC-1P or by grafting of (3-aminopropyl)silyl groups to the IPC-1P precursor preliminarily pillared with tetraethoxysilane (TEOS) were compared. The use of a mixture of aminosilsesquioxanes and TEOS for pillaring of IPC-1P led to the formation of functionalized materials, which are characterized by excellent textural properties (S-BET=154-435m(2)g(-1), V-total=0.336-0.630cm(3)g(-1)) and provide a 100% yield of target benzylidenemalononitrile in the Knoevenagel cond

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CF - Physical chemistry and theoretical chemistry

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GP13-17593P" target="_blank" >GP13-17593P: Preparation of Novel Structure-Directing Agents for the Synthesis of Zeolites</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2015

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    ChemPlusChem

  • ISSN

    2192-6506

  • e-ISSN

  • Volume of the periodical

    80

  • Issue of the periodical within the volume

    3

  • Country of publishing house

    DE - GERMANY

  • Number of pages

    7

  • Pages from-to

    599-605

  • UT code for WoS article

    000350471700021

  • EID of the result in the Scopus database

    2-s2.0-84922773276