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LiNi(1)(/)(3)Mn(1)(/)(3)Co(1)(/)(3)O(2)with morphology optimized for novel concept of3DLi accumulator

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388955%3A_____%2F20%3A00531781" target="_blank" >RIV/61388955:_____/20:00531781 - isvavai.cz</a>

  • Result on the web

    <a href="http://hdl.handle.net/11104/0310398" target="_blank" >http://hdl.handle.net/11104/0310398</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/er.5630" target="_blank" >10.1002/er.5630</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    LiNi(1)(/)(3)Mn(1)(/)(3)Co(1)(/)(3)O(2)with morphology optimized for novel concept of3DLi accumulator

  • Original language description

    An array of LiNi1/3Mn1/3Co1/3O2(NMC 111) samples with a hollow-sphere morphology enabling the use of binder-free, millimeter-thick electrodes in a battery are prepared by a combination of ball milling, hydrothermal treatment and calcination. Materials are studied by powder X-ray diffraction, nitrogen adsorption measurements, X-ray fluorescence analysis, and scanning electron microscopy. Their electrochemical performance for Li(+)extraction/insertion is tested by cyclic voltammetry and galvanostatic chronopotentiometry on thin-film electrodes. Optimized materials, prepared by mechanical and thermal treatment with surface areas of 7 to 10 m(2)g(-1), provide charge capacity values of 141 to 156 mAh g(-1). The concentration of the crystalline phase in NMC 111 materials with a hollow-sphere morphology is found to be the decisive parameter for their galvanostatic cycling stability. Hollow spheres with well-developed NMC nanocrystals and a low concentration of amorphous phase in the walls, exhibiting excellent cycling stability and charge capacity in thin-film electrodes are incorporated into a NMC/graphite 3D-battery module. This 122 Ah/451 Wh 3D-battery provides 78% of theoretical capacity and 73% of theoretical energy after 10 formatting cycles. Additionally, the battery prototype exhibits stable performance over more than 200 cycles at C/10 rate. A series of analogous 3D Li accumulators, currently assembled and tested in a pilot plant, represent the first step toward large-scale production of novel 3D Li accumulator.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10403 - Physical chemistry

Result continuities

  • Project

    <a href="/en/project/FV20471" target="_blank" >FV20471: Research and Construction Design of 48V Lithium Accumulators for New Generation of Automobiles</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2020

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    International Journal of Energy Research

  • ISSN

    0363-907X

  • e-ISSN

  • Volume of the periodical

    44

  • Issue of the periodical within the volume

    JUN 2020

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    11

  • Pages from-to

    9082-9092

  • UT code for WoS article

    000542450100001

  • EID of the result in the Scopus database

    2-s2.0-85087306250