Milling Activation for the Solvent-Free Synthesis of the Zeolite Mordenite
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388955%3A_____%2F20%3A00532025" target="_blank" >RIV/61388955:_____/20:00532025 - isvavai.cz</a>
Result on the web
<a href="http://hdl.handle.net/11104/0310627" target="_blank" >http://hdl.handle.net/11104/0310627</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1002/ejic.202000320" target="_blank" >10.1002/ejic.202000320</a>
Alternative languages
Result language
angličtina
Original language name
Milling Activation for the Solvent-Free Synthesis of the Zeolite Mordenite
Original language description
Milling by a planetary mill was applied as a pretreatment of a reagent mixture for the solvent-free synthesis of the zeolite mordenite. This method was compared with both manual grinding and standard hydrothermal synthesis. The comprehensive characterization of the obtained products was complemented by thorough studies of activated synthesis mixtures before crystallization steps (by Magic Angle Spinning Nuclear Magnetic Resonance and Scanning Electron Microscopy). This experimental approach gave insight into processes behind the synthesis mixture activation by milling. The characteristics of solvent-free zeolite product were comparable with material obtained by the classic hydrothermal route. The automated milling activation made the crystallization possible due to higher energetic impact in comparison to manual grinding. The solvent-free process allowed minimization of the contribution of water to a role of the agent catalyzing silica transformation, as a result, less than 5 % water (compared to the classical synthesis) was necessary to perform the crystallization.
Czech name
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Czech description
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Classification
Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10403 - Physical chemistry
Result continuities
Project
Result was created during the realization of more than one project. More information in the Projects tab.
Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Others
Publication year
2020
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
European Journal of Inorganic Chemistry
ISSN
1434-1948
e-ISSN
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Volume of the periodical
2020
Issue of the periodical within the volume
29
Country of publishing house
DE - GERMANY
Number of pages
7
Pages from-to
2791-2797
UT code for WoS article
000543974100001
EID of the result in the Scopus database
2-s2.0-85087155243