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Nature and Redox Properties of Iron Sites in Zeolites Revealed by Mossbauer Spectroscopy

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388955%3A_____%2F24%3A00580141" target="_blank" >RIV/61388955:_____/24:00580141 - isvavai.cz</a>

  • Result on the web

    <a href="https://hdl.handle.net/11104/0348907" target="_blank" >https://hdl.handle.net/11104/0348907</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/cplu.202300543" target="_blank" >10.1002/cplu.202300543</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Nature and Redox Properties of Iron Sites in Zeolites Revealed by Mossbauer Spectroscopy

  • Original language description

    Iron-containing zeolite-based catalysts play a pivotal role in environmental processes aimed at mitigating the release of harmful greenhouse gases, such as nitrous oxide (N2O) and methane (CH4). Despite the rich iron chemistry in zeolites, only a fraction of iron species that exhibit an open coordination sphere and possess the ability for electron transfer are responsible for activating reagents. In addition, the splitting of molecular oxygen is facilitated by bare iron cations embedded in zeolitic matrices. Mössbauer spectroscopy is the ideal tool for investigating the valency and geometry of iron species in zeolites because it leaves no iron forms silent and provides insights into in-situ processes. This review is dedicated to the utilization of Mössbauer spectroscopy to elucidate the nature of the extra-framework iron centers in ferrierite (FER), beta-structured (*BEA), and ZSM-5 zeolite (MFI) zeolites, which are active in N2O decomposition and CH4 oxidation through using the active oxygen derived from N2O and O-2. In this work, a structured summary of the Mössbauer parameters established over the last two decades is presented, characterizing the specific iron active centers and intermediates formed upon iron's interaction with N2O/O-2 and CH4. Additionally, the impact of preparation methods, iron loading, and the long-term stability on iron speciation and its redox behavior under reaction conditions is discussed.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10403 - Physical chemistry

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2024

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    ChemPlusChem

  • ISSN

    2192-6506

  • e-ISSN

    2192-6506

  • Volume of the periodical

    89

  • Issue of the periodical within the volume

    5

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    19

  • Pages from-to

    e202300543

  • UT code for WoS article

    001116949500001

  • EID of the result in the Scopus database

    2-s2.0-85178900991