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Photooxidation of Aniline Derivatives Can Be Activated by Freezing Their Aqueous Solutions

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388963%3A_____%2F17%3A00483886" target="_blank" >RIV/61388963:_____/17:00483886 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216224:14310/17:00095495

  • Result on the web

    <a href="http://dx.doi.org/10.1021/acs.est.7b04510" target="_blank" >http://dx.doi.org/10.1021/acs.est.7b04510</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1021/acs.est.7b04510" target="_blank" >10.1021/acs.est.7b04510</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Photooxidation of Aniline Derivatives Can Be Activated by Freezing Their Aqueous Solutions

  • Original language description

    A combined experimental and computational approach was, used to investigate the spectroscopic properties of three different aniline derivatives (aniline, N,N-dimethylaniline, and N,N-diethylaniline) in aqueous solutions and at the air-ice interface in the temperature range of 243-298 K The absorption and diffuse reflectance spectra of ice samples prepared by different techniques, such as slow or shock freezing of the aqueous solutions or vapor deposition on ice grains, exhibited unequivocal bathochromic shifts of 10-15 nm of the absorption maxima of anilines in frozen samples compared to those in liquid aqueous solutions. DFT and SCS-ADC(2) calculations showed that contaminant contaminant and contaminant-ice interactions are responsible for these shifts. Finally, we demonstrate that irradiation of anilines in the presence of a hydrogen peroxide/O-2 system by wavelengths that overlap only with the red-shifted absorption tails of anilines in frozen samples (while having a marginal overlap with their spectra in liquid solutions) can almost exclusively trigger a photochemical oxidation process. Mechanistic and environmental considerations are discussed.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10403 - Physical chemistry

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2017

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Environmental Science and Technology

  • ISSN

    0013-936X

  • e-ISSN

  • Volume of the periodical

    51

  • Issue of the periodical within the volume

    23

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    8

  • Pages from-to

    13763-13770

  • UT code for WoS article

    000417549500026

  • EID of the result in the Scopus database

    2-s2.0-85038206874