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Analysis of low concentration of free ferric oxides in clays by vis diffuse reflectance spectroscopy and voltammetry.

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388980%3A_____%2F02%3A50023035" target="_blank" >RIV/61388980:_____/02:50023035 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Analysis of low concentration of free ferric oxides in clays by vis diffuse reflectance spectroscopy and voltammetry.

  • Original language description

    Ferric oxide admixtures in the concentration range 0.1-10% in soils, sediments, and clay mineral samples can be conveniently characterized by Vis diffuse reflectance spectroscopy (DRS) in the region of d-d electron transitions close to 500 tint, voltammetry of microparticles, and voltatmmetry with carbon paste electroactive electrode (CPEE). DRS also detects Fe(Ill) in the clay mineral matrix equally sensitively. Voltammetry of microparticles is suitable for direct detection of free crystalline and amorphous ferric oxides, The determination limit of total free ferric oxides with CPEE is -0.01%. The techniques were tested with six clay mineral samples. XRD was able to detect free FeOOH in only one of them (1.6%). DRS and CPEE also detected 0.19% FeOOH in Be-3 (bentonite of Rokle deposit, Bohemia) and,C 0.04% in reference montmorillonite SWy-2.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CA - Inorganic chemistry

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GA205%2F00%2F1349" target="_blank" >GA205/00/1349: Detailed magnetic characteristics of power-plant fly ashes</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2002

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Geologica Carpathica

  • ISSN

    0016-7738

  • e-ISSN

  • Volume of the periodical

    53

  • Issue of the periodical within the volume

    2

  • Country of publishing house

    SK - SLOVAKIA

  • Number of pages

    7

  • Pages from-to

    71-77

  • UT code for WoS article

  • EID of the result in the Scopus database