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Mesoporous iron?manganese oxides for sulphur mustard and soman degradation

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388980%3A_____%2F12%3A00382564" target="_blank" >RIV/61388980:_____/12:00382564 - isvavai.cz</a>

  • Result on the web

    <a href="http://dx.doi.org/10.1016/j.materresbull.2012.09.015" target="_blank" >http://dx.doi.org/10.1016/j.materresbull.2012.09.015</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.materresbull.2012.09.015" target="_blank" >10.1016/j.materresbull.2012.09.015</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Mesoporous iron?manganese oxides for sulphur mustard and soman degradation

  • Original language description

    Substituted iron(III)?manganese(III, IV) oxides, ammonio-jarosite and birnessite, were prepared by a homogeneous hydrolysis of potassium permanganate and iron(III) sulphate with 2-chloroacetamide and urea, respectively. Synthesised oxides were characterised using Brunauer?Emmett?Teller (BET) surface area and Barrett?Joiner?Halenda porosity (BJH), X-ray diffraction (XRD), infrared spectroscopy (IR), Raman spectroscopy and scanning electron microscopy (SEM). The oxides were taken for an experimental evaluation of their reactivity against sulphur mustard (HD) and soman (GD). When ammonio-jarosite formation is suppressed by adding urea to the reaction mixture, the reaction products are mixtures of goethite, schwertmannite and ferrihydrite, and their degradation activity against soman considerably increases. The best activities for the degradation of sulphur mustard (97.9% in 64 min) and soman (97.9% in 64 min) were observed for FeMn_75 with 32.6 wt.% Fe (36.8 wt.% Mn) and FeMn_37U with 60.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CA - Inorganic chemistry

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GAP106%2F12%2F1116" target="_blank" >GAP106/12/1116: Nanocrystalline metal oxides for safe and fast degradation of organophosphorus pesticides</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2012

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Materials Research Bulletin

  • ISSN

    0025-5408

  • e-ISSN

  • Volume of the periodical

    47

  • Issue of the periodical within the volume

    12

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    9

  • Pages from-to

    4291-4299

  • UT code for WoS article

    000313851200059

  • EID of the result in the Scopus database