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Gamma radiolytic stability of CyMe4BTBP and effect of nitric acid

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388980%3A_____%2F15%3A00454290" target="_blank" >RIV/61388980:_____/15:00454290 - isvavai.cz</a>

  • Alternative codes found

    RIV/61388980:_____/15:00473536

  • Result on the web

    <a href="http://dx.doi.org/10.1515/nuka-2015-0156" target="_blank" >http://dx.doi.org/10.1515/nuka-2015-0156</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1515/nuka-2015-0156" target="_blank" >10.1515/nuka-2015-0156</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Gamma radiolytic stability of CyMe4BTBP and effect of nitric acid

  • Original language description

    The highly selective nitrogen donor ligand CyMe4BTBP for An(III) separation by solvent extraction was irradiated in a 60Co γ-source under varying conditions. Organic solutions of 10 mmol/L ligand in 1 octanol were contacted with different concentrations of nitric acid to observe the influence of an aqueous phase during irradiation. In subsequent liquid-liquid extraction experiments, distribution ratios of 241Am and 152Eu were determined. Distribution ratios decreased with increasing absorbed dose when irradiation was performed in the absence of nitric acid. With addition of nitric acid, initial distribution ratios remained constant over the whole examined dose range up to 300 kGy. For qualitative determination of radiolysis products, HPLC-MS measurements were performed. The protective effect of nitric acid was confirmed, since in samples irradiated with acid contact, no degradation products were observed, but only addition products of the α-hydroxy octyl radical to the CyMe4BTBP molecule.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10402 - Inorganic and nuclear chemistry

Result continuities

  • Project

    <a href="/en/project/7G13003" target="_blank" >7G13003: Safety of ACtinide Separation proceSSes</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2015

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Nukleonika

  • ISSN

    0029-5922

  • e-ISSN

  • Volume of the periodical

    60

  • Issue of the periodical within the volume

    4

  • Country of publishing house

    PL - POLAND

  • Number of pages

    6

  • Pages from-to

    879-884

  • UT code for WoS article

    000446055400012

  • EID of the result in the Scopus database

    2-s2.0-84957588069