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Development of Energy-Efficient ”Cold” Curing Method for Polypropylene Glycol Fumarate Using an Optimized Initiating System

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388980%3A_____%2F23%3A00570765" target="_blank" >RIV/61388980:_____/23:00570765 - isvavai.cz</a>

  • Result on the web

    <a href="https://hdl.handle.net/11104/0342102" target="_blank" >https://hdl.handle.net/11104/0342102</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.31489/2959-0663/1-23-10" target="_blank" >10.31489/2959-0663/1-23-10</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Development of Energy-Efficient ”Cold” Curing Method for Polypropylene Glycol Fumarate Using an Optimized Initiating System

  • Original language description

    The possibility of using the polymeric matrix obtained as a result of “cold” polymerization of polypropylene glycol fumarate (p-PGF) with methacrylic acid (MAA) as a polymeric base for obtaining new adhesives of domestic production was demonstrated. The starting reagent (p-PGF) was synthesized by condensation polymerization of fumaric acid with propylene glycol in the presence of a catalyst, which reduced the temperature and shortened the process time. A number of solutions of p-PGF in MAA of different mass compositions were obtained and their rheological properties were determined. Curing of the studied solutions was carried out by radical polymerization at room temperature in the presence of the “cold curing” initiating system. The optimum composition and amount of components of the “cold” curing initiating system consisting of an initiator (benzoyl peroxide) and a promoter (dimethylaniline) were established. Technological parameters of curing (temperature, lifetime and curing time, the value of volume shrinkage) were determined. The obtained compounds were identified by infrared spectroscopy. The surface morphology of the cured samples was studied by scanning electron microscopy. It was found that varying the composition of the initial polymermonomer mixture allows controlling the physicochemical properties.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10402 - Inorganic and nuclear chemistry

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2023

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Eurasian Journal of Chemistry

  • ISSN

    2959-0663

  • e-ISSN

    2959-0671

  • Volume of the periodical

    109

  • Issue of the periodical within the volume

    1

  • Country of publishing house

    KZ - KAZAKSTAN

  • Number of pages

    10

  • Pages from-to

    68-77

  • UT code for WoS article

    000944808400001

  • EID of the result in the Scopus database

    2-s2.0-85152957888