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Controlling crystallization: a key factor during 3D printing with the advanced semicrystalline polymeric materials PEEK, PEKK 6002, and PEKK 7002

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61389013%3A_____%2F23%3A00573952" target="_blank" >RIV/61389013:_____/23:00573952 - isvavai.cz</a>

  • Result on the web

    <a href="https://onlinelibrary.wiley.com/doi/10.1002/mame.202200668" target="_blank" >https://onlinelibrary.wiley.com/doi/10.1002/mame.202200668</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/mame.202200668" target="_blank" >10.1002/mame.202200668</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Controlling crystallization: a key factor during 3D printing with the advanced semicrystalline polymeric materials PEEK, PEKK 6002, and PEKK 7002

  • Original language description

    Controlling the crystallization of advanced, high-performance polymeric materials during 3D printing is critical to ensure that the resulting structures have appropriate mechanical properties. In this work, two grades of polyetherketoneketone (PEKK 6002 and PEKK 7002) are used to print 3D specimens via a fused filament fabrication process. The samples are compared with polyetheretherketone printed under the same conditions. Two approaches for controlling the crystallization process are undertaken. The first involves adjustment of the chamber temperature between room temperature and 190 °C to create two regions where crystallization is governed by the slow diffusion process and elevated by limiting the nucleation process. The second approach involves selection of PEKK materials with varying crystallization kinetics, namely. Application of this method into 3D-printing process allows for printing semicrystalline materials with tailored mechanical, thermal, and chemical properties as either amorphous or in situ crystallized products. The studies undertaken here provide the basis to eliminate expensive and time-consuming post-processing of 3D fabricated parts. In particular, solutions for the avoidance of poor adhesion to the building plate and weak interlayer adhesion that can lead to warping are described. The materials are divided into three groups, slow, moderate, and too fast crystallization kinetics.n

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10404 - Polymer science

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2023

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Macromolecular Materials and Engineering

  • ISSN

    1438-7492

  • e-ISSN

    1439-2054

  • Volume of the periodical

    308

  • Issue of the periodical within the volume

    7

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    10

  • Pages from-to

    2200668

  • UT code for WoS article

    000942755500001

  • EID of the result in the Scopus database

    2-s2.0-85149268914