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The effects of the deacetylation of chitin nanowhiskers on the performance of PCL/PLA bio-nanocomposites

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61389013%3A_____%2F23%3A00574964" target="_blank" >RIV/61389013:_____/23:00574964 - isvavai.cz</a>

  • Result on the web

    <a href="https://www.mdpi.com/2073-4360/15/14/3071" target="_blank" >https://www.mdpi.com/2073-4360/15/14/3071</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.3390/polym15143071" target="_blank" >10.3390/polym15143071</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    The effects of the deacetylation of chitin nanowhiskers on the performance of PCL/PLA bio-nanocomposites

  • Original language description

    The multiple roles of organic nanofillers in biodegradable nanocomposites (NC) with a blend-based matrix is not yet fully understood. This work highlights combination of reinforcing and structure-directing effects of chitin nanowhiskers (CNW) with different degrees of deacetylation (DA), i.e., content of primary or secondary amines on their surface, in the nanocomposite with the PCL/PLA 1:1 matrix. Of importance is the fact that aminolysis with CNW leading to chain scission of both polyesters, especially of PLA, is practically independent of DA. DA also does not influence thermal stability. At the same time, the more marked chain scission/CNW grafting for PLA in comparison to PCL, causing changes in rheological parameters of components and related structural alterations, has crucial effects on mechanical properties in systems with a bicontinuous structure. Favourable combinations of multiple effects of CNW leads to enhanced mechanical performance at low 1% content only, whereas negative effects of structural changes, particularly of changed continuity, may eliminate the reinforcing effects of CNW at higher contents. The explanation of both synergistic and antagonistic effects of structures formed is based on the correspondence of experimental results with respective basic model calculations.n

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10404 - Polymer science

Result continuities

  • Project

    <a href="/en/project/LUAUS23004" target="_blank" >LUAUS23004: Nanotubular materials from natural polymers for medical applications</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2023

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Polymers

  • ISSN

    2073-4360

  • e-ISSN

    2073-4360

  • Volume of the periodical

    15

  • Issue of the periodical within the volume

    14

  • Country of publishing house

    CH - SWITZERLAND

  • Number of pages

    15

  • Pages from-to

    3071

  • UT code for WoS article

    001037499000001

  • EID of the result in the Scopus database

    2-s2.0-85166326028