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Correlation of thermal and electrical properties of silver germanophosphate glasses with their structural analysis by Raman and NMR spectroscopy

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61389021%3A_____%2F24%3A00617087" target="_blank" >RIV/61389021:_____/24:00617087 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216275:25310/24:39921729

  • Result on the web

    <a href="https://www.sciencedirect.com/science/article/pii/S0254058424004826?via%3Dihub" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0254058424004826?via%3Dihub</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.matchemphys.2024.129357" target="_blank" >10.1016/j.matchemphys.2024.129357</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Correlation of thermal and electrical properties of silver germanophosphate glasses with their structural analysis by Raman and NMR spectroscopy

  • Original language description

    In present study glasses of the system Ag2O-GeO2-P2O5 were studied in the compositional series (50−x)Ag2O-xGeO2-50P2O5 with x = 0−40 mol%. Ag2O substitution by GeO2 results in a significant increase of both glass transition temperature, Tg, and crystallization temperature, Tc, up to 628 °C (Tg) and 851 °C (Tc) at x = 40 mol% GeO2. The glass structure was investigated from the analysis of 31P MAS NMR and Raman spectra. Both methods show transformation of phosphate glass network formed mainly by Q2 units to germanate-phosphate network formed by Q1xGe and Q21Ge phosphate units and germanate units. Raman spectra, in addition, reveal evolution of P‒O‒P linkages to P‒O‒Ge and Ge‒O‒Ge linkages through the glass series. DC conductivity trend upon GeO2 addition showed non-monotonic behaviour, which is related to structural changes in the glass-network.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10302 - Condensed matter physics (including formerly solid state physics, supercond.)

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2024

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Materials Chemistry and Physics

  • ISSN

    0254-0584

  • e-ISSN

    1879-3312

  • Volume of the periodical

    319

  • Issue of the periodical within the volume

    June

  • Country of publishing house

    NL - THE KINGDOM OF THE NETHERLANDS

  • Number of pages

    10

  • Pages from-to

    129357

  • UT code for WoS article

    001220440700001

  • EID of the result in the Scopus database

    2-s2.0-85190865830