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Microwave-Assisted Synthesis, Characterization and Tribological Properties of a g-C3N4/MoS2 Nanocomposite for Low Friction Coatings

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989100%3A27230%2F22%3A10251476" target="_blank" >RIV/61989100:27230/22:10251476 - isvavai.cz</a>

  • Result on the web

    <a href="https://www.mdpi.com/2079-6412/12/12/1840" target="_blank" >https://www.mdpi.com/2079-6412/12/12/1840</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.3390/coatings12121840" target="_blank" >10.3390/coatings12121840</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Microwave-Assisted Synthesis, Characterization and Tribological Properties of a g-C3N4/MoS2 Nanocomposite for Low Friction Coatings

  • Original language description

    This study explores the tribological performance of microwave-assisted synthesized g-C3N4/MoS2 coatings. The two-dimensional transition metal dichalcogenide (TMD) nanosheet is getting prominence in the study of tribology due to its layered structure. The graphitic carbon nitride (g-C3N4) nanosheet was made using the calcination method and its nanocomposite with molybdenum disulfide (MoS2) was produced using a microwave-assisted method. The structure and morphology of the samples were characterized by some well-known methods, and tribological properties were studied by a pin-on-disc (POD) apparatus. Morphological analysis revealed that graphitic carbon nitride and molybdenum disulfide coexisted, and the layer structured MoS2 was well dispersed on graphitic carbon nitride nanosheets. BET analysis was used to determine the pore volume and specific surface area of the synthesized materials. The inclusion of MoS2 nanoparticles caused the composite&apos;s pore volume and specific surface area to decrease. The reduction in g-C3N4 pore volume and specific surface area confirmed that the pores of calcinated graphitic carbon nitride were filled with MoS2 nanoparticles. The tribological property of g-C3N4/MoS2 nanocomposite was systematically investigated under different factors such as applied loads (5N to 15N), sliding speed (500 to 1000 mm/s) and material composition (uncoated, MoS2-coated, 9 wt.% of g-C3N4 and 20 wt.% of g-C3N4 in the composite). The optimal composite material ratio was taken 9%, by weight of g-C3N4 in the g-C3N4/MoS2 composite for a variety of levels of loads and sliding speeds. The results indicates that the incorporation of g-C3N4 in nanocomposites could reduce friction and improve wear life, which were better than the results with single MoS2. This study demonstrates a solution to broaden the possible uses of g-C3N4 and MoS2-based materials in the field of tribology. (C) 2022 by the authors.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    20301 - Mechanical engineering

Result continuities

  • Project

    <a href="/en/project/EF17_049%2F0008407" target="_blank" >EF17_049/0008407: Innovative and additive manufacturing technology - new technological solutions for 3D printing of metals and composite materials</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2022

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Coatings

  • ISSN

    2079-6412

  • e-ISSN

    2079-6412

  • Volume of the periodical

    12

  • Issue of the periodical within the volume

    12

  • Country of publishing house

    CH - SWITZERLAND

  • Number of pages

    16

  • Pages from-to

    nestrankovano

  • UT code for WoS article

    000900560100001

  • EID of the result in the Scopus database

    2-s2.0-85144875798