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Nanocomposite of montmorillonite and silver nanoparticles: characterization and application for catalytic reduction of 4-nitrophenol

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989100%3A27360%2F13%3A86088373" target="_blank" >RIV/61989100:27360/13:86088373 - isvavai.cz</a>

  • Result on the web

    <a href="http://dx.doi.org/10.1016/j.matchemphys.2013.03.059" target="_blank" >http://dx.doi.org/10.1016/j.matchemphys.2013.03.059</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.matchemphys.2013.03.059" target="_blank" >10.1016/j.matchemphys.2013.03.059</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Nanocomposite of montmorillonite and silver nanoparticles: characterization and application for catalytic reduction of 4-nitrophenol

  • Original language description

    Silver ions previously intercalated into a montmorillonite (MMT) interlayer were reduced by sodium borohydride forming a nanocomposite of MMT and silver nanoparticles (Ag-MMT) with no other stabilizing additives. Within 360 min no coagulation of an aqueous Ag-MMT dispersion was observed. However, after 24 h the coagulation was indicated by a red shift of absorption maximum from 408 nm to 434 nm and by broadening of the absorbance band. The nanocomposite was characterized by transmission electron microscopy (TEM), X-ray powder diffraction (XRD) and measurements of specific surface area (SSA). It contained 4.94 wt. % of silver. Ag nanoparticles with an average size of 6.9 nm were located on the external MMTsurface, mostly in its pores. Ag-MMT was used asa catalyst for reduction of 4-nitrophenol with sodium borohydride forming 4-aminophenol. After 30 s the reaction kinetics changed from zero order to first order, which was explained by means of the LangmuireHinshelwood model. The whole r

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    JI - Composite materials

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/ED0040%2F01%2F01" target="_blank" >ED0040/01/01: Regional materials science and technology centre</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2013

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Materials Chemistry and Physics

  • ISSN

    0254-0584

  • e-ISSN

  • Volume of the periodical

    140

  • Issue of the periodical within the volume

    2-3

  • Country of publishing house

    CH - SWITZERLAND

  • Number of pages

    6

  • Pages from-to

    493-498

  • UT code for WoS article

    000320837700012

  • EID of the result in the Scopus database