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Polyaniline as a precursor of multi-layer graphene: Microscopic and microspectroscopic study

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989100%3A27360%2F19%3A10239533" target="_blank" >RIV/61989100:27360/19:10239533 - isvavai.cz</a>

  • Alternative codes found

    RIV/61989100:27640/19:10239533 RIV/61989100:27740/19:10239533

  • Result on the web

    <a href="https://www.ingentaconnect.com/contentone/asp/jnn/2019/00000019/00000012/art00030" target="_blank" >https://www.ingentaconnect.com/contentone/asp/jnn/2019/00000019/00000012/art00030</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1166/jnn.2019.15878" target="_blank" >10.1166/jnn.2019.15878</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Polyaniline as a precursor of multi-layer graphene: Microscopic and microspectroscopic study

  • Original language description

    Aluminosilicate-based nanocomposites containing multi-layer graphene were prepared from polyaniline/montmorillonite intercalate in two different forms: tablets and thin layers. Starting materials, polyaniline/montmorillonite powder and polyaniline/montmorillonite layers deposited on quartz glass, were prepared by in situ polymerization of aniline in presence of montmorillonite particles.Powder was compacted into tablets using pressure 400 MPa. Samples were calcined at 1300 oC in argon atmosphere and multi-layer graphene was formed from polyaniline in both cases as confirmed by Raman microspectroscopy. Changes in morphology and surface conductivity of uncalcined and calcined samples were observed using atomic force microscopy and conductive atomic force microscopy. Also the differences between surface and internal volume of tablets were studied. Conductive atomic force microscopy revealed that the most conductive areas can be found solely on the edges of aluminosilicate particles formed from montmorillonite during calcination process. Detailed observation of multi-layer graphene in these areas was performed using transmission electron microscopy.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    21001 - Nano-materials (production and properties)

Result continuities

  • Project

    <a href="/en/project/LQ1602" target="_blank" >LQ1602: IT4Innovations excellence in science</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>S - Specificky vyzkum na vysokych skolach

Others

  • Publication year

    2019

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Journal of nanoscience and nanotechnology

  • ISSN

    1533-4880

  • e-ISSN

  • Volume of the periodical

    19

  • Issue of the periodical within the volume

    12

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    12

  • Pages from-to

    "7736–7747"

  • UT code for WoS article

    000473105800030

  • EID of the result in the Scopus database