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In vitro safety signals for potential clinical development of the anti-inflammatory pregnane X receptor agonist FKK6

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989592%3A15110%2F24%3A73625408" target="_blank" >RIV/61989592:15110/24:73625408 - isvavai.cz</a>

  • Alternative codes found

    RIV/61989592:15640/24:73625408 RIV/61989592:15310/24:73625408 RIV/00027006:_____/24:10177145

  • Result on the web

    <a href="https://www.sciencedirect.com/science/article/pii/S0045206824000427" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0045206824000427</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.bioorg.2024.107137" target="_blank" >10.1016/j.bioorg.2024.107137</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    In vitro safety signals for potential clinical development of the anti-inflammatory pregnane X receptor agonist FKK6

  • Original language description

    Based on the mimicry of microbial metabolites, functionalized indoles were demonstrated as the ligands and agonists of the pregnane X receptor (PXR). The lead indole, FKK6, displayed PXR-dependent protective effects in DSS-induced colitis in mice and in vitro cytokine-treated intestinal organoid cultures. Here, we report on the initial in vitro pharmacological profiling of FKK6. FKK6-PXR interactions were characterized by hydrogen–deuterium exchange mass spectrometry. Screening FKK6 against potential cellular off-targets (G protein-coupled receptors, steroid and nuclear receptors, ion channels, and xenobiotic membrane transporters) revealed high PXR selectivity. FKK6 has poor aqueous solubility but was highly soluble in simulated gastric and intestinal fluids. A large fraction of FKK6 was bound to plasma proteins and chemically stable in plasma. The partition coefficient of FKK6 was 2.70, and FKK6 moderately partitioned into red blood cells. In Caco2 cells, FKK6 displayed high permeability (A-B: 22.8 × 10–6 cm.s−1) and no active efflux. These data are indicative of essentially complete in vivo absorption of FKK6. The data from human liver microsomes indicated that FKK6 is rapidly metabolized by cytochromes P450 (t1/2 5 min), notably by CYP3A4. Two oxidized FKK6 derivatives, including DC73 (N6-oxide) and DC97 (C19-phenol), were detected, and these metabolites had 5–7 × lower potency as PXR agonists than FKK6. This implies that despite high intestinal absorption, FKK6 is rapidly eliminated by the liver, and its PXR effects are predicted to be predominantly in the intestines. In conclusion, the PXR ligand and agonist FKK6 has a suitable pharmacological profile supporting its potential preclinical development.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10608 - Biochemistry and molecular biology

Result continuities

  • Project

    <a href="/en/project/GA22-00355S" target="_blank" >GA22-00355S: Pharmacological mimicry of microbial metabolites in the modulation of intestinal health</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2024

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    BIOORGANIC CHEMISTRY

  • ISSN

    0045-2068

  • e-ISSN

    1090-2120

  • Volume of the periodical

    144

  • Issue of the periodical within the volume

    MAR

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    12

  • Pages from-to

    "107137-1107137"-"1107137-12"

  • UT code for WoS article

    001167691400001

  • EID of the result in the Scopus database

    2-s2.0-85183622015