5-Substituted 6-azauracils XVII. Synthesis of 5-(m-tolyl)-6-azauracil
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989592%3A15310%2F00%3A00000982" target="_blank" >RIV/61989592:15310/00:00000982 - isvavai.cz</a>
Result on the web
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DOI - Digital Object Identifier
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Alternative languages
Result language
angličtina
Original language name
5-Substituted 6-azauracils XVII. Synthesis of 5-(m-tolyl)-6-azauracil
Original language description
7-Methylisatin (I) was converted to appropriate senicarbazone. Its alkaline recyklization afforded 5-(2-amino-3-methyl)-6-azauracil. Its diazotation and subsequent redictive elimination of diazonium group led to the 5-(m-tolyl)-6-azauracil. Reaction of diazotated amine with ethyl cyanoacetylcarbamate afforded appropriate hydrazone. After reaction with bicarbonate this compound was converted to 1-[2-(6-azauracil-5-yl)-6-methylphenyl]-6-azauracil-5-carbonitrile. Cyclization of 5-(2-amino-3-methyl)-6-azauracil afforded 3,5-dihydro-5H-6-methyl-[1,2,4]-triazino[5,6-b]indole-3-one.
Czech name
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Czech description
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Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CC - Organic chemistry
OECD FORD branch
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Result continuities
Project
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Continuities
Z - Vyzkumny zamer (s odkazem do CEZ)
Others
Publication year
2000
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Acta Universitatis Palackianae Olomucensis, Facultas Rerum Naturalium, Chemica
ISSN
0232-0061
e-ISSN
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Volume of the periodical
39
Issue of the periodical within the volume
NA
Country of publishing house
XX - stateless person
Number of pages
6
Pages from-to
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UT code for WoS article
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EID of the result in the Scopus database
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