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Activation of alpha-Fe2O3 for Photoelectrochemical Water Splitting Strongly Enhanced by Low Temperature Annealing in Low Oxygen Containing Ambient

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989592%3A15310%2F20%3A73601471" target="_blank" >RIV/61989592:15310/20:73601471 - isvavai.cz</a>

  • Result on the web

    <a href="https://chemistry-europe.onlinelibrary.wiley.com/doi/full/10.1002/chem.201904430" target="_blank" >https://chemistry-europe.onlinelibrary.wiley.com/doi/full/10.1002/chem.201904430</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/chem.201904430" target="_blank" >10.1002/chem.201904430</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Activation of alpha-Fe2O3 for Photoelectrochemical Water Splitting Strongly Enhanced by Low Temperature Annealing in Low Oxygen Containing Ambient

  • Original language description

    Photoelectrochemical (PEC) water splitting is a promising method for the conversion of solar energy into chemical energy stored in the form of hydrogen. Nanostructured hematite (alpha-Fe2O3) is one of the most attractive materials for a highly efficient charge carrier generation and collection due to its large specific surface area and the short minority carrier diffusion length. In the present work, the PEC water splitting performance of nanostructured alpha-Fe2O3 is investigated which was prepared by anodization followed by annealing in a low oxygen ambient (0.03 % O-2 in Ar). It was found that low oxygen annealing can activate a significant PEC response of alpha-Fe2O3 even at a low temperature of 400 degrees C and provide an excellent PEC performance compared with classic air annealing. The photocurrent of the alpha-Fe2O3 annealed in the low oxygen at 1.5 V vs. RHE results as 0.5 mA cm(-2), being 20 times higher than that of annealing in air. The obtained results show that the alpha-Fe2O3 annealed in low oxygen contains beneficial defects and promotes the transport of holes; it can be attributed to the improvement of conductivity due to the introduction of suitable oxygen vacancies in the alpha-Fe2O3. Additionally, we demonstrate the photocurrent of alpha-Fe2O3 annealed in low oxygen ambient can be further enhanced by Zn-Co LDH, which is a co-catalyst of oxygen evolution reaction. This indicates low oxygen annealing generates a promising method to obtain an excellent PEC water splitting performance from alpha-Fe2O3 photoanodes.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10405 - Electrochemistry (dry cells, batteries, fuel cells, corrosion metals, electrolysis)

Result continuities

  • Project

    <a href="/en/project/EF15_003%2F0000416" target="_blank" >EF15_003/0000416: Advanced Hybrid Nanostructures for Renewable Energy Applications</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2020

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    CHEMISTRY-A EUROPEAN JOURNAL

  • ISSN

    0947-6539

  • e-ISSN

  • Volume of the periodical

    26

  • Issue of the periodical within the volume

    12

  • Country of publishing house

    DE - GERMANY

  • Number of pages

    8

  • Pages from-to

    2685-2692

  • UT code for WoS article

    000512441800001

  • EID of the result in the Scopus database

    2-s2.0-85079443568