Simultaneous determination of ten anticoagulant rodenticides in tissues by column-switching UHPLC-ESI-MS/MS
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F62157124%3A16270%2F15%3A43873776" target="_blank" >RIV/62157124:16270/15:43873776 - isvavai.cz</a>
Result on the web
<a href="http://dx.doi.org/10.1007/s00216-015-8954-1" target="_blank" >http://dx.doi.org/10.1007/s00216-015-8954-1</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1007/s00216-015-8954-1" target="_blank" >10.1007/s00216-015-8954-1</a>
Alternative languages
Result language
angličtina
Original language name
Simultaneous determination of ten anticoagulant rodenticides in tissues by column-switching UHPLC-ESI-MS/MS
Original language description
This paper describes the development of a method for the simultaneous determination of ten anticoagulant rodenticides (coumafuryl, warfarin, pindone, coumatetralyl, coumachlor, difenacoum, bromadiolone, brodifacoum, chlorophacinone and flocoumafen) in the liver and kidney based on column-switching liquid chromatography coupled with heated electrospray ionization tandem mass spectrometry. The simple sample preparation includes extraction with methanol. A C-18 trapping column was used for online solid-phase extraction before analytical separation with the mobile phase comprising a mixture of 0.1 % formic acid in water, methanol and acetonitrile. Chromatographic separation was achieved using a Thermo Hypersil ultra high-performance liquid chromatography (UHPLC) C-18 column with the mobile phase consisting of 5 mM ammonium formate buffer (pH = 9) and methanol. The column-switching procedure ensured no matrix effects during electrospray ionization (ESI). Extraction recoveries ranged between
Czech name
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Czech description
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Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
GJ - Diseases and animal vermin, veterinary medicine
OECD FORD branch
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Result continuities
Project
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Continuities
N - Vyzkumna aktivita podporovana z neverejnych zdroju
Others
Publication year
2015
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Analytical and Bioanalytical Chemistry
ISSN
1618-2642
e-ISSN
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Volume of the periodical
407
Issue of the periodical within the volume
25
Country of publishing house
US - UNITED STATES
Number of pages
6
Pages from-to
7849-7854
UT code for WoS article
000361633700031
EID of the result in the Scopus database
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