Ethylacetate synthesis by coupling of fixed bed reactor and reactive distillation-process integration aspects

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F62243136%3A_____%2F09%3A%230000120" target="_blank" >RIV/62243136:_____/09:#0000120 - isvavai.cz</a>
Result on the web
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DOI - Digital Object Identifier
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Result language
angličtina
Original language name
Ethylacetate synthesis by coupling of fixed bed reactor and reactive distillation-process integration aspects
Original language description
Coupling of a fixed-bed reactor and a reactive distillation column was used for acetic acid and ethanol esterification utilizing strong acidic ion-exchange resin as catalyst. Laboratory experiments were focussed on the investigation of catalyst loading effect on reaction conversion in a fixed-bed reactor at the temperature interval between 60 and 120 °C with partial separation of products in the form of their azeotropic mixture by the flash distillation. This procedure increased the reaction conversionabove chemical equilibrium. The experimental results achieved with a reactive distillation column of the overall efficiency of 14 theoretical stages (1 reaction stage) were successfully compared with numerical simulation by means of AspenPlus software.
Czech name
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Czech description
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Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CI - Industrial chemistry and chemical engineering
OECD FORD branch
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Project
<a href="/en/project/FT-TA3%2F074" target="_blank" >FT-TA3/074: *Utilization of vegetable oils and glycerin for the production of motor fuels.</a><br>
Continuities
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Publication year
2009
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

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